图谱信息 供应商 相关产品
网站主页CAS数据库列表 78-69-3更多图谱四氢芳樟醇(78-69-3)核磁图(1HNMR)

四氢芳樟醇

产品名称 四氢芳樟醇

CAS号78-69-3

分子式C10H22O

分子量158.28

展开


  • Mass

    MS-NW-7073          
    3,7-dimethyl-3-octanol
    C10H22O             (Mass of molecular ion:    158)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       5.2
          28.0       2.7
          29.0       7.0
          31.0       2.2
          39.0       3.5
          41.0      11.3
          42.0       2.1
          43.0      15.9
          45.0       5.6
          53.0       1.2
          55.0      26.7
          56.0       3.0
          57.0       5.1
          58.0       2.3
          59.0       1.9
          69.0      47.2
          70.0       7.9
          71.0       2.9
          72.0       2.6
          73.0     100.0
          74.0       4.6
          83.0       4.5
          84.0       1.0
          85.0       1.3
         111.0       9.6
         112.0       1.0
         125.0       1.3
         129.0       7.1
         143.0       2.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H22 O 0.05 ml : 0.5 ml CDCl3
    3,7-dimethyl-3-octanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.551 B 1.481 C 1.42 D 1.41 E 1.32 F 1.17 G 1.141 J 0.890 K 0.879 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

        633.91   1.587     30
        627.20   1.570     63
        620.61   1.553     81
        613.89   1.537     71
        607.18   1.520     42
        604.00   1.512     67
        596.44   1.493    212
        588.87   1.474    239
        581.42   1.455     95
        573.00   1.434     60
        570.68   1.428     71
        567.02   1.419    306
        562.87   1.409     84
        558.84   1.399     72
        555.79   1.391    172
        550.29   1.377     30
        541.63   1.356     44
        540.53   1.353     43
        538.21   1.347     35
        533.57   1.336     72
        530.40   1.328     57
        528.81   1.324     57
        525.63   1.316     73
        524.90   1.314     75
        522.95   1.309     62
        520.87   1.304     46
        518.80   1.299     43
        517.70   1.296     49
        515.87   1.291     47
        513.31   1.285     30
        508.91   1.274     33
        478.39   1.198     87
        471.92   1.181    128
        470.09   1.177     95
        468.14   1.172     56
        464.23   1.162    104
        463.26   1.160    110
        461.43   1.155     46
        456.05   1.142    815
        363.28   0.909    299
        360.72   0.903     45
        355.71   0.891    784
        354.86   0.888    978
        348.27   0.872   1000
    

in CDCl3



liquid film



4880 A,200 M,liquid