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MS-NW-2107 triethyl orthoacetate C8H18O3 (Mass of molecular ion: 162)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 3.8 15.0 9.4 18.0 1.4 19.0 2.9 26.0 6.8 27.0 34.7 28.0 9.7 29.0 59.5 30.0 3.5 31.0 72.6 41.0 3.3 42.0 54.9 43.0 100.0 44.0 4.0 45.0 57.8 46.0 12.7 47.0 1.0 59.0 2.3 60.0 95.9 61.0 45.7 62.0 1.4 63.0 1.1 70.0 5.2 71.0 1.7 72.0 1.1 73.0 3.0 87.0 4.2 88.0 2.3 89.0 16.7 116.0 30.8 117.0 11.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H18 O3 0.04 ml : 0.5 ml CDCl3 triethyl orthoacetate Assign. Shift(ppm)
A 3.541 B 1.463 C 1.205
Hz ppm Int.
328.13 3.664 129 321.00 3.585 474 313.88 3.505 506 306.88 3.427 159 131.00 1.463 750 117.50 1.312 21 114.75 1.282 507 112.69 1.259 46 110.56 1.235 36 109.94 1.228 26 107.69 1.203 1000 100.56 1.123 434
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