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1-辛烷磺酰氯

CAS号7795-95-1

分子式C8H17ClO2S

分子量212.74

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  • Mass

    MS-NW-2940          
    1-octanesulfonyl chloride
    C8H17ClO2S          (Mass of molecular ion:    212)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.3
          18.0       1.4
          26.0       1.5
          27.0      23.7
          28.0       5.7
          29.0      37.6
          36.0       4.3
          38.0       1.4
          39.0      16.6
          40.0       3.3
          41.0      76.5
          42.0      38.1
          43.0      82.6
          44.0       3.0
          48.0       5.3
          50.0       1.6
          51.0       2.6
          52.0       1.9
          53.0       4.2
          54.0       5.1
          55.0      80.9
          56.0      66.8
          57.0      56.8
          58.0       2.7
          63.0       2.2
          64.0      11.0
          67.0       6.9
          68.0      20.3
          69.0     100.0
          70.0      46.8
          71.0      29.2
          72.0       1.7
          77.0       3.9
          78.0       8.9
          79.0       1.2
          81.0       3.1
          82.0       7.8
          83.0      35.9
          84.0      34.5
          85.0       4.4
          91.0       3.3
          93.0       1.0
          95.0       1.0
          97.0       6.1
         105.0       1.1
         109.0       5.2
         110.0       1.9
         111.0      10.8
         112.0       8.2
         113.0       1.2
         114.0       1.2
         159.0       4.8
         177.0       2.8
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H17 Cl O2 S 0.05 ml : 0.5 ml CDCl3
    1-octanesulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.65 B 2.05 C 1.59 to 1.23 D 0.90

         Hz     ppm     Int.
    

        335.38   3.745    434
        332.06   3.708     36
        329.75   3.682    203
        327.88   3.662    389
        325.25   3.632    186
        319.94   3.573    595
        197.88   2.210     36
        197.56   2.206     35
        197.19   2.202     37
        195.94   2.188     34
        195.56   2.184     34
        195.25   2.181     32
        194.88   2.176     34
        194.31   2.170     36
        190.44   2.127    115
        190.06   2.123    117
        189.00   2.111    106
        187.63   2.096    103
        186.81   2.086    109
        185.06   2.067    132
        182.81   2.042    176
        180.69   2.018    128
        179.31   2.003    132
        175.13   1.956    148
        173.13   1.934    114
        170.56   1.905     50
        169.81   1.897     49
        167.56   1.871     78
        149.63   1.671     31
        149.06   1.665     33
        148.00   1.653     36
        147.25   1.645     39
        146.69   1.638     40
        145.81   1.629     44
        145.44   1.624     45
        144.69   1.616     46
        140.00   1.564    114
        139.19   1.555    116
        138.69   1.549    116
        138.19   1.543    127
        135.75   1.516    131
        135.31   1.511    134
        134.69   1.504    138
        133.00   1.486    171
        131.56   1.469    206
        117.69   1.315    989
        115.19   1.287   1000
        101.81   1.137     50
        101.13   1.130     47
        100.81   1.126     46
         99.44   1.111     43
         99.13   1.107     42
         98.81   1.104     41
         97.44   1.088     33
         97.06   1.084     32
         96.63   1.079     31
         95.94   1.072     31
         95.50   1.067     31
         93.75   1.047     32
         93.25   1.042     33
         92.06   1.028     42
         91.50   1.022     43
         91.25   1.019     43
         90.81   1.014     44
         84.75   0.947    246
         79.63   0.890    776
         73.50   0.821    168
         69.75   0.779     61
    

in CDCl3



liquid film