邻羟基苯乙醇

Mass

MS-NW-7408          
2-hydroxyphenethyl alcohol
C8H10O2             (Mass of molecular ion:    138)

   Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       3.2
      28.0       2.9
      29.0       1.6
      31.0       3.0
      38.0       1.6
      39.0       8.0
      40.0       1.2
      41.0       1.1
      43.0       1.0
      50.0       3.1
      51.0       7.2
      52.0       3.6
      53.0       4.6
      55.0       1.5
      62.0       1.5
      63.0       3.9
      64.0       1.4
      65.0       5.0
      66.0       1.2
      74.0       1.0
      75.0       1.0
      77.0      28.6
      78.0       6.4
      79.0      15.3
      80.0       2.3
      89.0       3.1
      90.0       4.9
      91.0      17.3
      92.0       4.8
      94.0       1.4
     107.0     100.0
     108.0      21.5
     109.0       1.8
     119.0       7.3
     120.0      33.8
     121.0       3.6
     138.0      37.8
     139.0       3.7

Assign. Shift(ppm) A 7.03 B 6.98 C 6.81 D 6.80 E 3.791 F 2.784 B,C,D AND E WERE CONFIRMED BY LAOCN PROGRAM. UNUSUAL BASE LINE IS CAUSED BY OH.

     Hz     ppm     Int.

    645.92   7.213     31
    645.41   7.207     33
    644.68   7.199     33
    644.38   7.195     32
    643.87   7.190     36
    640.80   7.155    230
    638.82   7.133    161
    636.84   7.111     86
    633.54   7.074    340
    632.15   7.059    460
    630.69   7.043    423
    629.74   7.032    372
    626.88   7.000    304
    624.68   6.975    818
    623.51   6.962    897
    615.45   6.872    318
    613.99   6.856    824
    612.30   6.837    786
    610.40   6.816    470
    608.35   6.793    461
    607.47   6.783    521
    604.61   6.751    407
    602.93   6.733    240
    600.88   6.710    196
    599.41   6.693    155
    596.85   6.665     38
    595.83   6.653     36
    595.02   6.644     30
    345.12   3.854    549
    339.55   3.792   1000
    333.76   3.727    707
    328.27   3.666     49
    327.17   3.654     43
    326.81   3.650     37
    326.00   3.641     34
    325.71   3.637     33
    325.12   3.631     32
    324.83   3.627     32
    324.17   3.620     32
    260.52   2.909     32
    255.03   2.848    586
    249.39   2.785    827
    243.75   2.722    471
    236.57   2.642     35
    235.40   2.629     31