-
MassMS-NW-6665 1,1,3,3-tetramethyl-1,3-divinyldisilazane C8H19NSi2 (Mass of molecular ion: 185)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
28.0 1.3 31.0 1.4 43.0 3.9 44.0 1.7 45.0 4.5 50.5 1.5 51.5 3.1 55.0 1.2 57.5 2.8 58.0 1.2 58.5 5.7 59.0 14.8 60.0 4.4 61.0 1.4 63.5 7.1 64.0 1.6 64.5 4.8 65.0 1.0 70.0 2.6 71.0 2.7 71.5 1.1 72.0 1.5 73.0 13.4 74.0 9.2 75.0 1.5 77.5 3.2 83.0 1.2 85.0 5.1 86.0 4.0 87.0 2.1 99.0 1.0 100.0 7.6 101.0 1.1 102.0 6.4 103.0 1.2 104.0 1.0 112.0 1.3 114.0 1.4 116.0 26.5 117.0 5.7 118.0 5.8 119.0 1.2 128.0 7.8 129.0 1.6 130.0 16.8 131.0 2.8 132.0 3.2 142.0 40.7 143.0 7.7 144.0 5.6 145.0 1.1 153.0 1.1 154.0 2.8 156.0 1.2 158.0 15.2 159.0 3.2 160.0 1.4 168.0 2.9 170.0 100.0 171.0 21.2 172.0 8.6 173.0 1.2 185.0 2.2
400 MHz in CDCl3
-
1H NMR 399.65 MHz C8 H19 N Si2 0.05 ml : 0.5 ml CDCl3 1,1,3,3-tetramethyl-1,3-divinyldisilazane 
Assign. Shift(ppm)
A 6.140 B 5.906 C 5.697 D 0.126
Hz ppm Int.2473.51 6.190 133 2458.74 6.153 173 2453.25 6.139 163 2438.60 6.102 214 2368.90 5.928 201 2364.87 5.918 223 2354.25 5.891 165 2350.22 5.881 167 2288.09 5.726 200 2284.18 5.716 187 2267.94 5.675 166 2263.92 5.665 157 62.01 0.156 25 61.28 0.154 24 53.96 0.136 202 50.42 0.127 1000 47.12 0.118 291 40.28 0.101 55
in CDCl3
liquid film
更多供应商
