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MS-IW-9541 p-tert-butylaniline C10H15N (Mass of molecular ion: 149)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.4 28.0 1.9 29.0 1.1 39.0 4.3 41.0 5.1 51.0 1.9 52.0 1.4 53.0 1.4 58.5 2.2 63.0 1.5 65.0 5.2 65.5 2.1 66.0 3.0 67.0 1.9 77.0 5.0 78.0 1.4 79.0 1.3 89.0 1.0 91.0 4.9 92.0 1.3 93.0 9.5 94.0 15.6 95.0 1.1 105.0 1.0 106.0 16.1 107.0 1.6 115.0 1.3 117.0 3.5 118.0 5.6 119.0 6.1 120.0 1.0 132.0 1.6 133.0 2.3 134.0 100.0 135.0 10.3 149.0 22.7 150.0 2.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H15 N 0.05 ml : 0.5 ml CDCl3 p-tert-butylaniline Assign. Shift(ppm)
A 7.164 B 6.598 C 3.50 D 1.266
Hz ppm Int.
2870.24 7.182 34 2867.43 7.175 197 2865.23 7.170 73 2860.96 7.159 81 2858.76 7.154 199 2855.96 7.147 28 2643.92 6.616 38 2641.11 6.609 215 2638.92 6.604 75 2634.52 6.593 78 2632.57 6.588 190 2629.52 6.580 26 1396.97 3.496 44 519.53 1.300 24 506.10 1.267 1000 0.00 0.001 73
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