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MassMS-NW-7284 n-cyclohexylformamide C7H13NO (Mass of molecular ion: 127)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 6.9 28.0 10.8 29.0 5.1 30.0 7.3 39.0 8.0 40.0 1.5 41.0 13.4 42.0 8.9 43.0 15.9 44.0 2.0 46.0 100.0 47.0 1.9 51.0 1.5 53.0 3.3 54.0 11.3 55.0 7.3 56.0 39.1 57.0 3.2 58.0 4.0 59.0 3.0 67.0 23.7 68.0 2.3 69.0 1.1 70.0 4.5 71.0 8.5 72.0 1.6 79.0 1.8 81.0 5.2 82.0 17.9 83.0 1.9 84.0 59.1 85.0 4.3 98.0 5.5 99.0 2.2 112.0 1.6 126.0 1.6 127.0 8.6 128.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H13 N O 0.034 g : 0.5 ml CDCl3 N-cyclohexylformamide 
Assign. Shift(ppm)
A 8.13 A 8.10 B 6.2 B 6.0 C 3.851 C 3.302 D 1.92 E 1.72 F 1.62 G 1.37 J 1.31 K 1.20 MIXTURE OF INTERNAL ROTATIONAL ISOMERS
Hz ppm Int.3248.29 8.128 316 3236.08 8.098 1000 3234.38 8.094 883 2490.72 6.233 31 2401.86 6.010 104 1552.98 3.886 112 1548.71 3.876 123 1545.53 3.868 166 1544.31 3.865 156 1542.11 3.859 230 1538.09 3.849 216 1533.94 3.839 227 1532.10 3.834 158 1531.01 3.831 167 1527.59 3.823 121 1523.07 3.812 109 777.10 1.945 440 773.80 1.937 455 764.53 1.913 485 760.86 1.904 565 699.10 1.750 490 695.43 1.741 523 691.41 1.731 377 685.55 1.716 421 681.64 1.706 539 677.98 1.697 389 556.52 1.393 362 552.98 1.384 583 542.97 1.359 476 541.02 1.354 570 539.55 1.351 579 531.01 1.329 489 527.71 1.321 437 521.85 1.306 396 493.53 1.235 350 490.11 1.227 352 488.53 1.223 395 481.08 1.204 603 479.13 1.199 657 476.81 1.194 627 470.46 1.178 552 467.41 1.170 587 463.87 1.161 420
in CDCl3
liquid film
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