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网站主页CAS数据库列表 766-93-8更多图谱N-环己基甲酰氨(766-93-8)核磁图(13CNMR)

N-环己基甲酰氨

产品名称 N-环己基甲酰氨

CAS号766-93-8

分子式C7H13NO

分子量127.18

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  • Mass

    MS-NW-7284          
    n-cyclohexylformamide
    C7H13NO             (Mass of molecular ion:    127)
    

       Source Temperature: 210 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       6.9
          28.0      10.8
          29.0       5.1
          30.0       7.3
          39.0       8.0
          40.0       1.5
          41.0      13.4
          42.0       8.9
          43.0      15.9
          44.0       2.0
          46.0     100.0
          47.0       1.9
          51.0       1.5
          53.0       3.3
          54.0      11.3
          55.0       7.3
          56.0      39.1
          57.0       3.2
          58.0       4.0
          59.0       3.0
          67.0      23.7
          68.0       2.3
          69.0       1.1
          70.0       4.5
          71.0       8.5
          72.0       1.6
          79.0       1.8
          81.0       5.2
          82.0      17.9
          83.0       1.9
          84.0      59.1
          85.0       4.3
          98.0       5.5
          99.0       2.2
         112.0       1.6
         126.0       1.6
         127.0       8.6
         128.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H13 N O 0.034 g : 0.5 ml CDCl3
    N-cyclohexylformamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.13 A 8.10 B 6.2 B 6.0 C 3.851 C 3.302 D 1.92 E 1.72 F 1.62 G 1.37 J 1.31 K 1.20 MIXTURE OF INTERNAL ROTATIONAL ISOMERS

         Hz     ppm     Int.
    

       3248.29   8.128    316
       3236.08   8.098   1000
       3234.38   8.094    883
       2490.72   6.233     31
       2401.86   6.010    104
       1552.98   3.886    112
       1548.71   3.876    123
       1545.53   3.868    166
       1544.31   3.865    156
       1542.11   3.859    230
       1538.09   3.849    216
       1533.94   3.839    227
       1532.10   3.834    158
       1531.01   3.831    167
       1527.59   3.823    121
       1523.07   3.812    109
        777.10   1.945    440
        773.80   1.937    455
        764.53   1.913    485
        760.86   1.904    565
        699.10   1.750    490
        695.43   1.741    523
        691.41   1.731    377
        685.55   1.716    421
        681.64   1.706    539
        677.98   1.697    389
        556.52   1.393    362
        552.98   1.384    583
        542.97   1.359    476
        541.02   1.354    570
        539.55   1.351    579
        531.01   1.329    489
        527.71   1.321    437
        521.85   1.306    396
        493.53   1.235    350
        490.11   1.227    352
        488.53   1.223    395
        481.08   1.204    603
        479.13   1.199    657
        476.81   1.194    627
        470.46   1.178    552
        467.41   1.170    587
        463.87   1.161    420
    

in CDCl3



liquid film