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网站主页CAS数据库列表 76350-90-8更多图谱3-羟甲基-2-甲基联苯(76350-90-8)红外图谱(IR2)

3-羟甲基-2-甲基联苯

产品名称 3-羟甲基-2-甲基联苯

CAS号76350-90-8

分子式C14H14O

分子量198.26

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  • Mass

    MS2015-05117CW      
    (2-methyl-3-biphenylyl)methanol
    C14H14O             (Mass of molecular ion:    198)
    

       Source Temperature: 245 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          28.0       1.2
          39.0       1.8
          51.0       2.8
          63.0       2.9
          65.0       2.1
          74.0       1.0
          75.0       1.5
          76.0       4.3
          77.0       6.4
          78.0       1.2
          82.0       1.5
          82.5       3.1
          87.0       1.2
          88.0       1.4
          89.0       9.8
          90.0       2.6
          91.0       4.9
          91.5       1.0
          93.0       1.3
          98.0       1.1
         102.0       1.8
         113.0       1.0
         115.0       7.4
         116.0       1.0
         121.0       1.0
         126.0       1.7
         127.0       3.0
         128.0       5.7
         129.0       2.5
         139.0       4.8
         141.0       3.6
         150.0       1.3
         151.0       4.6
         152.0      22.8
         153.0      12.1
         154.0      10.8
         155.0      26.6
         156.0       3.5
         163.0       3.0
         164.0       3.8
         165.0     100.0
         166.0      21.1
         167.0      14.5
         168.0       2.7
         169.0      10.2
         170.0       1.5
         176.0       2.3
         177.0       2.1
         178.0      15.7
         179.0      38.4
         180.0      71.1
         181.0      12.4
         182.0       2.0
         183.0      11.6
         184.0       1.7
         196.0       1.3
         197.0       1.9
         198.0      69.4
         199.0      10.5
    

in DMSO-d6

400 MHz in CDCl3




  • 1H NMR 399.65 MHz
    C14 H14 O 0.038 g : 0.5 ml CDCl3
    (2-methyl-3-biphenylyl)methanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.39 B 7.37 C 7.336 D 7.279 E 7.237 F 7.188 G 4.729 J 2.215 K 1.94

         Hz     ppm     Int.
    

       2965.45   7.421     69
       2964.11   7.417    123
       2962.52   7.413     57
       2959.11   7.405     82
       2957.28   7.400    272
       2955.69   7.396    184
       2953.49   7.391     41
       2951.17   7.385    134
       2949.83   7.382    329
       2948.97   7.379    256
       2941.77   7.361    122
       2940.67   7.359    126
       2938.72   7.354     95
       2937.26   7.350    158
       2935.79   7.346    109
       2932.37   7.338     58
       2929.81   7.331    153
       2927.25   7.325     48
       2924.07   7.317     39
       2922.61   7.313     59
       2921.14   7.310     33
       2913.09   7.290    274
       2911.50   7.286    362
       2909.30   7.280     91
       2906.37   7.273    130
       2904.79   7.269    238
       2903.44   7.265    182
       2900.88   7.259     89
       2893.07   7.240    165
       2876.22   7.197    145
       2874.76   7.194    152
       2868.53   7.178     78
       2867.19   7.175     71
       1890.26   4.730    463
        885.50   2.216   1000
        776.98   1.945     85
    

in DMSO-d6

in CDCl3





KBr disc



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