4-溴-2-氟苄溴

产品名称 4-溴-2-氟苄溴

CAS号76283-09-5

分子式C7H5Br2F

分子量267.92

¹³CNMR

Mass

MS-KW-0080          
4-bromo-1-bromomethyl-2-fluorobenzene
C7H5Br2F            (Mass of molecular ion:    266)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      31.0       2.0
      38.0       1.4
      39.0       1.9
      44.0       3.5
      50.0       2.8
      51.0       1.9
      53.0       1.4
      54.0       2.7
      56.0       1.0
      57.0       5.5
      61.0       1.7
      62.0       3.6
      63.0       3.6
      74.0       1.0
      79.0       1.4
      80.0       3.1
      81.0       6.2
      82.0       3.8
      83.0       3.1
      84.0       2.8
      86.0       1.0
      87.0       1.1
      89.0       1.1
      93.0       1.6
      93.5       2.0
      94.0       1.6
      94.5       1.9
     106.0       1.0
     107.0      19.3
     108.0      36.2
     109.0       3.3
     123.0       1.7
     124.0       3.4
     125.0       1.6
     134.0       1.2
     187.0     100.0
     188.0       8.5
     189.0      97.1
     190.0       7.9
     266.0       4.1
     268.0       8.0
     270.0       3.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₅ Br₂ F	0.038 g : 0.5 ml CDCl₃
4-bromo-1-bromomethyl-2-fluorobenzene

    Assign.     Shift(ppm)

      A          7.28 to 7.25
      B             4.455

     Hz     ppm     Int.

   2915.89   7.297     60
   2914.31   7.293     69
   2908.69   7.279    485
   2907.71   7.276    955
   2906.13   7.272    494
   2902.34   7.263    307
   2899.29   7.255     34
   2896.97   7.249    217
   2895.39   7.245    205
   2894.04   7.242    111
   1781.25   4.458   1000
   1780.15   4.455    872

in CDCl3

KBr disk

Nujol

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4-溴-2-氟苄溴(76283-09-5)质谱(MS) 相关产品图谱

溴化乙啶(1239-45-8)质谱(MS) 溴化乙啶(1239-45-8)红外图谱(IR1) 溴化乙啶(1239-45-8)红外图谱(IR2) 溴化乙啶(1239-45-8)核磁图(¹HNMR) 二氟溴乙酸乙酯(667-27-6)核磁图(¹³CNMR)

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