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MassMS-NW-4908 2,2,3,3-tetrafluoro-1-propanol C3H4F4O (Mass of molecular ion: 132)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
18.0 1.7 28.0 2.5 29.0 18.6 30.0 1.5 31.0 100.0 32.0 2.5 33.0 8.3 43.0 1.2 44.0 1.2 45.0 3.1 49.0 7.0 51.0 18.8 61.0 3.8 63.0 1.4 64.0 3.1 65.0 6.2 81.0 1.2 82.0 26.7 83.0 1.8 112.0 8.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H4 F4 O 0.04 ml : 0.5 ml CDCl3 2,2,3,3-tetrafluoro-1-propanol 
Assign. Shift(ppm)
A 5.928 B 3.976 C 2.59 J2(A,F-19)=53.2HZ J3(A,F-19)=4.3HZ J3(B,F-19)=13.5HZ J4(B,F-19)=1.6HZ
Hz ppm Int.588.31 6.569 128 584.06 6.522 252 579.88 6.475 124 535.13 5.976 256 530.88 5.928 523 526.63 5.881 262 481.94 5.382 122 477.69 5.334 254 473.44 5.287 126 370.88 4.142 218 369.25 4.123 392 367.69 4.106 220 357.69 3.994 429 356.13 3.977 773 354.50 3.959 428 344.56 3.848 223 342.94 3.830 388 341.38 3.812 218 232.00 2.591 1000
CCl4 solution
liquid film
4880 A,200 M,liquid
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