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MassMS-NW-9953 3,5-dibromo-o-phenylenediamine monohydrochloride C6H6Br2N2 HCl (Mass of molecular ion: 264)
Source Temperature: 140 °C Sample Temperature: 90 °C Direct, 75 eV
17.0 2.7 18.0 14.8 28.0 4.7 35.0 1.9 36.0 25.1 37.0 1.2 38.0 8.4 50.0 3.2 51.0 5.7 52.0 9.4 52.5 2.8 53.0 9.1 54.0 1.3 61.0 1.0 62.0 1.9 63.0 1.0 65.0 1.3 75.0 1.2 76.0 4.6 77.0 2.3 78.0 10.3 79.0 4.8 80.0 1.6 82.0 1.4 89.0 1.8 92.0 1.5 92.5 1.2 93.0 1.7 93.5 1.2 103.0 1.0 105.0 10.5 106.0 13.0 107.0 1.0 132.0 2.4 133.0 4.4 134.0 2.0 156.0 1.1 157.0 1.2 158.0 6.7 159.0 1.5 160.0 5.6 168.0 2.4 170.0 2.4 183.0 1.0 184.0 2.4 185.0 10.9 186.0 3.5 187.0 9.7 188.0 1.1 236.0 1.8 238.0 3.5 240.0 1.7 263.0 1.9 264.0 51.2 265.0 7.4 266.0 100.0 267.0 9.2 268.0 48.7 269.0 3.6
parameter in DMSO-d6
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1H NMR 300 MHz C6 H6 Br2 N2 0.032 g : 0.5 ml DMSO-d6 3,5-dibromo-o-phenylenediamine monohydrochloride 
Parameter ppm Hz
D(A) 7.494 D(B) 7.352 J(A,B) 2.2 D(C) 6.2
Hz ppm Int.2249.33 7.498 911 2247.14 7.490 1000 2206.67 7.356 1000 2204.48 7.348 911 1859.98 6.200 73
KBr disc
nujol mull
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