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MS-IW-6976 trimethylvinylsilane C5H12Si (Mass of molecular ion: 100)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 2.6 31.0 2.5 42.0 1.7 43.0 10.8 44.0 2.0 45.0 7.4 53.0 2.4 55.0 3.2 57.0 1.3 58.0 3.7 59.0 64.6 60.0 4.9 61.0 2.2 72.0 7.0 73.0 13.5 74.0 1.3 85.0 100.0 86.0 9.7 87.0 3.9 100.0 8.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H12 Si 0.05 ml : 0.5 ml CDCl3 trimethylvinylsilane Assign. Shift(ppm)
A 6.156 B 5.919 C 5.666 D 0.071
Hz ppm Int.
2479.49 6.205 91 2464.84 6.168 117 2459.23 6.154 105 2444.58 6.117 139 2374.02 5.941 126 2370.12 5.931 138 2359.38 5.904 101 2355.47 5.894 101 2275.51 5.694 121 2271.61 5.684 112 2255.13 5.643 100 2251.34 5.634 94 38.94 0.098 21 31.62 0.080 252 28.56 0.072 1000 24.90 0.063 184
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