硼烷-三甲胺络合物

产品名称硼烷-三甲胺络合物

CAS号75-22-9

分子式C3H12BN

分子量72.95

¹³CNMR

Mass

MS-NW-8856          
borane-trimethylamine complex
C3H9N H3B           (Mass of molecular ion:     73)

   Source Temperature: 280 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      13.0       1.7
      15.0       4.6
      26.0       3.9
      27.0      13.1
      28.0      12.0
      29.0       6.6
      30.0      17.5
      39.0       2.3
      40.0       8.2
      41.0      14.2
      42.0      18.8
      43.0       3.3
      44.0       3.5
      53.0       2.8
      54.0      10.1
      55.0       8.4
      56.0      33.0
      57.0       3.3
      58.0      61.3
      59.0      22.6
      68.0       4.3
      69.0       7.1
      70.0      20.0
      71.0      30.8
      72.0     100.0
      73.0       4.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₃ H₉ N	0.041 g : 0.5 ml CDCl₃
borane-trimethylamine complex

    Assign.     Shift(ppm)

      A             2.664
      B             1.71

     Hz     ppm     Int.

   1064.94   2.665   1000

in CDCl3

KBr disc

nujol mull

4880 A,200 M,

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