-
MS-IW-1486 trans-5-decene C10H20 (Mass of molecular ion: 140)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 8.6 28.0 1.0 29.0 8.3 39.0 10.2 40.0 1.5 41.0 37.3 42.0 17.4 43.0 23.4 51.0 1.0 53.0 4.4 54.0 8.1 55.0 100.0 56.0 53.5 57.0 13.5 65.0 1.2 67.0 6.9 68.0 3.7 69.0 48.6 70.0 40.1 71.0 6.0 79.0 1.1 81.0 2.4 82.0 2.9 83.0 15.1 84.0 13.3 85.0 3.4 96.0 1.4 97.0 15.1 98.0 5.5 111.0 4.5 112.0 2.5 140.0 26.5 141.0 2.9
90 MHz in CDCl3
-
1H NMR 89.56 MHz C10 H20 0.05 ml : 0.5 ml CDCl3 trans-5-decene Assign. Shift(ppm)
A 5.387 B 1.97 C 1.35 D 1.25 E 0.89
Hz ppm Int.
487.75 5.447 132 486.19 5.429 251 484.13 5.406 242 482.50 5.388 394 480.94 5.371 239 478.94 5.348 262 477.31 5.330 135 186.50 2.083 93 185.94 2.077 96 179.63 2.006 277 178.19 1.990 282 177.19 1.979 270 174.50 1.949 304 170.00 1.899 162 169.69 1.895 160 163.44 1.825 44 162.63 1.816 39 162.06 1.810 37 161.50 1.804 37 160.81 1.796 35 159.81 1.785 32 138.06 1.542 32 137.06 1.531 33 136.13 1.520 39 135.69 1.516 42 134.06 1.497 53 132.25 1.477 70 131.13 1.465 63 127.00 1.419 223 122.88 1.373 415 119.69 1.337 715 116.94 1.306 644 115.94 1.295 634 112.31 1.255 470 109.44 1.222 266 106.69 1.192 145 105.56 1.179 130 105.25 1.176 131 102.06 1.140 67 100.31 1.121 93 99.13 1.107 70 97.56 1.090 73 94.88 1.060 51 93.88 1.049 48 92.50 1.033 64 92.19 1.030 63 91.56 1.023 65 85.81 0.959 403 85.06 0.950 373 83.50 0.933 323 79.44 0.888 1000 74.63 0.834 266 73.50 0.821 252 72.13 0.806 190 70.50 0.788 115 69.38 0.775 103
更多供应商