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MassMS-NW-7468 4-bromophenethylamine C8H10BrN (Mass of molecular ion: 199)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
18.0 2.0 28.0 2.1 30.0 100.0 31.0 1.4 39.0 1.6 50.0 1.2 51.0 1.5 63.0 2.4 65.0 1.0 77.0 1.0 89.0 3.6 90.0 4.1 91.0 2.8 106.0 1.1 169.0 1.5 171.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H10 Br N 0.05 ml : 0.5 ml CDCl3 4-bromophenethylamine 
Assign. Shift(ppm)
A 7.372 B 7.038 C 2.891 D 2.683 E 2.03
Hz ppm Int.674.38 7.530 32 670.81 7.491 54 668.00 7.459 135 665.69 7.433 563 663.69 7.411 253 659.19 7.361 365 657.25 7.339 865 654.88 7.313 199 647.44 7.230 32 647.13 7.226 32 646.81 7.223 30 646.44 7.218 30 635.81 7.100 212 633.63 7.075 757 631.50 7.052 266 629.31 7.027 112 627.06 7.002 246 625.44 6.984 439 625.00 6.979 462 622.63 6.953 106 620.44 6.928 48 619.63 6.919 42 618.94 6.911 38 618.50 6.906 34 617.56 6.896 31 617.19 6.892 30 269.00 3.004 114 266.56 2.977 143 263.38 2.941 179 260.06 2.904 476 255.06 2.848 435 254.00 2.837 456 250.44 2.797 87 244.63 2.732 435 241.31 2.695 141 238.69 2.666 445 235.50 2.630 180 232.31 2.594 136 229.75 2.566 106 227.69 2.543 36 227.06 2.536 32 191.25 2.136 30 190.31 2.125 34 182.06 2.033 1000 174.56 1.950 67 174.25 1.946 63 171.94 1.920 41 171.44 1.915 37 170.94 1.909 35 170.31 1.902 33 169.44 1.892 31
in CDCl3
liquid film
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