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MS-NW-9260 4-chloropyridine hydrochloride C5H4ClN HCl (Mass of molecular ion: 113)
Source Temperature: 150 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 1.6 26.0 1.1 28.0 1.7 35.0 2.4 36.0 34.3 37.0 1.6 38.0 11.5 38.5 1.7 49.0 3.0 50.0 11.1 51.0 24.6 52.0 2.6 56.5 1.1 60.0 1.5 73.0 2.6 75.0 1.9 76.0 4.0 77.0 1.5 78.0 65.3 79.0 3.9 85.0 1.5 86.0 4.3 87.0 1.0 88.0 1.4 112.0 1.6 113.0 100.0 114.0 8.1 115.0 32.2 116.0 2.4
90 MHz in D2O
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1H NMR 89.56 MHz C5 H4 Cl N 0.040 g : 0.5 ml D2O 4-chloropyridine hydrochloride Assign. Shift(ppm)
A 8.794 B 8.19 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.
791.81 8.842 768 790.63 8.828 357 790.06 8.822 335 786.63 8.784 353 784.75 8.763 1000 783.13 8.745 192 736.75 8.227 742 731.31 8.166 306 729.75 8.149 584
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