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网站主页CAS数据库列表 7370-92-5更多图谱四氢-6-辛基-2H-吡喃-2-酮(7370-92-5)红外图谱(IR1)

四氢-6-辛基-2H-吡喃-2-酮

产品名称 四氢-6-辛基-2H-吡喃-2-酮

CAS号7370-92-5

分子式C13H24O2

分子量212.33

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  • Mass

    MS-IW-3655          
    5-tridecanolide
    C13H24O2            (Mass of molecular ion:    212)
    

       Source Temperature: 210 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          27.0       6.2
          28.0       1.1
          29.0       8.2
          39.0       4.7
          40.0       1.0
          41.0      21.3
          42.0      18.3
          43.0      21.4
          44.0       1.3
          53.0       1.7
          54.0       3.3
          55.0      27.4
          56.0      12.7
          57.0       9.9
          58.0       1.5
          60.0       1.9
          67.0       4.5
          68.0       6.8
          69.0      15.5
          70.0      29.1
          71.0      28.2
          72.0       1.6
          73.0       2.9
          81.0       4.3
          82.0       4.2
          83.0       8.5
          84.0       6.9
          85.0       1.6
          86.0       3.0
          87.0       1.2
          95.0       3.0
          96.0       5.9
          97.0       8.2
          98.0       8.2
          99.0     100.0
         100.0       9.6
         101.0       2.1
         109.0       1.6
         110.0       4.0
         111.0       3.6
         112.0       1.8
         113.0       2.0
         114.0      13.2
         115.0       2.8
         123.0       1.9
         124.0       1.9
         125.0       1.8
         127.0       1.4
         134.0       1.8
         137.0       1.7
         138.0       1.0
         141.0       3.1
         142.0       1.4
         150.0       4.9
         151.0       1.9
         152.0       3.1
         176.0       1.8
         194.0       3.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H24 O2 0.05 ml : 0.5 ml CDCl3
    5-tridecanolide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.282 B 2.580 C 2.450 D 1.91 E 1.85 F *1 1.69 G *1 1.57 J *2 1.51 K *2 1.38 L 1.27 M 0.880

         Hz     ppm     Int.
    

       1721.80   4.309     52
       1719.60   4.303     54
       1717.16   4.297     85
       1713.87   4.289     77
       1712.04   4.284     71
       1710.82   4.281     80
       1709.11   4.277     84
       1706.42   4.270     79
       1703.61   4.263     54
       1701.42   4.258     52
       1042.11   2.608     75
       1035.64   2.592     54
       1031.62   2.582     83
       1030.40   2.579     66
       1026.61   2.569     83
       1024.41   2.564    109
       1023.32   2.561    101
       1019.65   2.552     53
       1018.07   2.548     76
        992.31   2.483    111
        985.23   2.466    113
        983.64   2.462    143
        976.56   2.444    101
        974.73   2.439     75
        967.65   2.422     55
        965.94   2.417     87
        958.86   2.400     51
        775.63   1.941     99
        774.17   1.938     89
        772.46   1.933    103
        770.87   1.929    141
        769.17   1.925    117
        765.50   1.916    152
        764.40   1.913    114
        761.96   1.907    143
        760.13   1.902    173
        758.67   1.899    157
        757.93   1.897    144
        756.59   1.894    165
        753.54   1.886    140
        751.95   1.882     73
        748.90   1.874    108
        744.87   1.864     67
        743.65   1.861     65
        742.55   1.859     72
        740.60   1.854     47
        738.65   1.849     55
        737.92   1.847     51
        736.94   1.844     58
        735.60   1.841     66
        734.13   1.837     67
        731.81   1.832     49
        726.93   1.819     54
        687.38   1.720     58
        686.04   1.717     63
        684.69   1.714     64
        681.27   1.705     83
        678.71   1.699     67
        677.25   1.695     79
        676.27   1.693     73
        673.95   1.687     79
        671.39   1.680     72
        668.95   1.674     62
        664.31   1.663     58
        647.09   1.620     55
        641.97   1.607     94
        636.84   1.594    134
        631.71   1.581    191
        628.30   1.573    115
        626.46   1.568    150
        623.54   1.561    147
        620.61   1.553    109
        618.29   1.548    168
        616.58   1.543    135
        613.89   1.537    160
        609.62   1.526    114
        608.64   1.523    126
        605.83   1.516    173
        603.15   1.510    137
        599.85   1.501    101
        598.14   1.497    111
        595.09   1.490    115
        593.26   1.485     86
        590.94   1.479     81
        589.23   1.475     68
        587.89   1.472     66
        586.06   1.467     59
        583.01   1.459     49
        559.08   1.399     52
        557.25   1.395     46
        554.20   1.387     65
        549.19   1.375     67
        546.88   1.369     60
        543.58   1.361     73
        511.47   1.280    906
        358.76   0.898    346
        352.05   0.881   1000
        344.97   0.864    399
    

in CDCl3



liquid film