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MassMS-NW-9662 N(4),1-dimethyl-4-piperidinamine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 3.0 18.0 1.5 27.0 4.1 28.0 7.6 29.0 4.2 30.0 6.0 39.0 3.4 41.0 6.5 42.0 38.4 43.0 59.1 44.0 29.9 45.0 1.0 52.0 1.0 53.0 2.0 54.0 4.4 55.0 13.2 56.0 14.3 57.0 12.7 58.0 11.2 67.0 1.2 68.0 8.6 69.0 4.4 70.0 34.3 71.0 17.7 72.0 2.2 79.0 1.1 80.0 1.0 81.0 1.8 82.0 27.3 83.0 2.3 84.0 6.5 85.0 3.4 94.0 2.6 96.0 64.1 97.0 100.0 98.0 12.8 99.0 3.7 128.0 4.5 129.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H16 N2 0.05 ml : 0.5 ml CDCl3 N(4),1-dimethyl-4-piperidinamine 
Assign. Shift(ppm)
A 2.805 B 2.427 C 2.329 D 2.263 E 1.987 F 1.873 G 1.379 J 1.23 ASSIGNED BY H-H COSY.
Hz ppm Int.1127.20 2.821 83 1118.16 2.798 61 1115.11 2.791 90 969.97 2.428 1000 942.14 2.358 35 935.79 2.342 40 931.76 2.332 68 927.73 2.322 44 925.54 2.316 32 921.39 2.306 38 908.45 2.274 68 904.42 2.264 950 807.13 2.020 55 804.81 2.014 63 795.41 1.991 102 793.21 1.985 116 783.81 1.962 56 781.62 1.956 64 757.69 1.896 67 756.84 1.894 72 755.49 1.891 77 754.15 1.888 73 752.93 1.884 71 749.02 1.875 49 745.12 1.865 75 744.02 1.862 81 742.55 1.859 86 741.33 1.855 80 740.36 1.853 77 569.82 1.426 39 566.04 1.417 40 558.35 1.398 67 557.01 1.394 72 555.66 1.391 71 554.57 1.388 75 546.63 1.368 67 545.65 1.366 65 544.19 1.362 66 542.72 1.358 63 535.03 1.339 30 531.25 1.330 30
in CDCl3
liquid film
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