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硼烷-叔丁基胺

产品名称 硼烷-叔丁基胺

CAS号7337-45-3

分子式C4H11BN

分子量83.94784

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  • Mass

    MS-NW-8841          
    borane-tert-butylamine complex
    C4H11N H3B          (Mass of molecular ion:     87)
    

       Source Temperature: 280 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          13.0       1.0
          15.0       4.0
          18.0      11.2
          26.0       1.6
          27.0       8.8
          28.0       9.8
          29.0      10.7
          30.0       7.1
          39.0       9.9
          40.0       3.1
          41.0      40.7
          42.0      30.5
          43.0      28.5
          44.0       1.2
          52.0       1.2
          53.0       1.3
          54.0       1.8
          55.0       3.4
          56.0       7.5
          57.0      28.2
          58.0     100.0
          59.0       3.8
          67.0       1.1
          68.0       3.9
          69.0      10.2
          70.0      40.5
          71.0       1.6
          86.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H11 N 0.037 g : 0.5 ml CDCl3
    borane-tert-butylamine complex
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.8 B 1.4 C 1.301

         Hz     ppm     Int.
    

       1527.59   3.823     23
        520.26   1.302   1000
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder