己二烯

Mass

MS-IW-3676          
trans-1,4-hexadiene
C6H10               (Mass of molecular ion:     82)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      26.0       2.6
      27.0      18.8
      28.0       3.8
      29.0       7.3
      37.0       1.7
      38.0       4.2
      39.0      42.9
      40.0       7.2
      41.0      55.5
      42.0       7.8
      43.0       1.3
      50.0       6.1
      51.0       8.6
      52.0       4.3
      53.0      22.9
      54.0      25.6
      55.0      13.2
      56.0       1.8
      63.0       1.8
      65.0      13.8
      66.0       4.3
      67.0     100.0
      68.0       7.7
      74.0       1.0
      77.0       5.3
      78.0       1.1
      79.0      11.5
      80.0       2.1
      81.0      16.0
      82.0      62.5
      83.0       4.3

Assign. Shift(ppm) A 5.807 B 5.45 C 5.44 D 5.01 E 4.97 F 2.722 G 1.660 J(A,D)=17.1HZ J(A,E)=10.1HZ J(A,F)=6.5HZ ASSIGNED BY H-H COSY.

     Hz     ppm     Int.

   2341.80   5.860    110
   2335.33   5.844    218
   2331.67   5.835    123
   2328.86   5.828    116
   2325.20   5.819    260
   2318.24   5.801    284
   2314.58   5.792    139
   2311.77   5.785    131
   2308.11   5.776    262
   2301.64   5.760    131
   2200.81   5.507     41
   2195.56   5.494     66
   2186.40   5.471     71
   2185.55   5.469    134
   2180.42   5.456    560
   2178.10   5.451    316
   2175.78   5.445    809
   2173.71   5.440    282
   2171.02   5.433    350
   2168.21   5.426     51
   2166.14   5.421     35
   2160.89   5.407     64
   2155.64   5.394     52
   2014.40   5.041    133
   2012.70   5.037    308
   2010.74   5.032    370
   2009.03   5.027    185
   1997.19   4.998    123
   1995.48   4.994    277
   1993.53   4.989    343
   1991.94   4.985    304
   1990.72   4.982    352
   1989.38   4.978    263
   1988.77   4.977    323
   1987.43   4.973    173
   1981.93   4.960    162
   1980.59   4.956    316
   1979.25   4.953    242
   1978.64   4.951    302
   1977.29   4.948    162
   1096.19   2.743    121
   1094.85   2.740    200
   1093.26   2.736    214
   1091.92   2.733    225
   1090.70   2.730    306
   1089.60   2.727    380
   1088.26   2.724    405
   1086.91   2.720    332
   1085.57   2.717    264
   1084.35   2.714    304
   1083.13   2.711    317
   1081.79   2.707    246
   1080.57   2.704    141
    671.02   1.680     38
    667.72   1.671    484
    666.38   1.668    918
    665.53   1.666    864
    665.16   1.665    861
    664.06   1.662    556
    662.96   1.659    646
    661.62   1.656   1000
    660.28   1.653    678