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MS-NW-7195 2-bromotricyclo(3.3.1.1(3,7))decane C10H15Br (Mass of molecular ion: 214)
Source Temperature: 210 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 3.3 29.0 1.7 39.0 6.2 41.0 6.2 51.0 2.2 52.0 1.3 53.0 3.2 55.0 3.7 65.0 3.5 66.0 1.7 67.0 17.0 68.0 1.0 69.0 2.5 77.0 6.4 78.0 2.3 79.0 15.1 80.0 2.2 81.0 9.1 91.0 5.7 92.0 2.5 93.0 14.4 94.0 1.2 105.0 1.3 107.0 3.6 135.0 100.0 136.0 11.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H15 Br 0.035 g : 0.5 ml CDCl3 2-bromotricyclo(3.3.1.1(3,7))decane Assign. Shift(ppm)
A 4.674 B 2.50 to 1.45
Hz ppm Int.
420.06 4.691 193 418.63 4.675 226 417.31 4.660 188 216.38 2.417 170 204.13 2.280 247 192.38 2.149 320 191.50 2.139 319 181.63 2.029 86 171.38 1.914 1000 159.75 1.784 560 154.69 1.728 296 152.44 1.703 306 151.38 1.691 308 138.31 1.545 200 137.19 1.532 217 131.44 1.468 26
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