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5-氯-2-硝基苯甲醇

产品名称 5-氯-2-硝基苯甲醇

CAS号73033-58-6

分子式C7H6ClNO3

分子量187.58

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  • Mass

    MS-NW-7884          
    5-chloro-2-nitrobenzyl alcohol
    C7H6ClNO3           (Mass of molecular ion:    187)
    

       Source Temperature: 140 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          17.0       1.0
          18.0       4.2
          26.0       1.2
          27.0       6.8
          28.0       7.1
          29.0      13.4
          30.0      11.4
          31.0      10.9
          36.0       1.6
          37.0       3.0
          38.0       7.0
          39.0      15.9
          40.0       1.3
          45.0       2.1
          47.0       6.5
          49.0       2.3
          50.0      27.4
          51.0      58.4
          52.0      11.6
          53.0       4.1
          55.0       2.9
          61.0       5.5
          62.0      11.8
          63.0      27.9
          64.0       4.9
          65.0      18.7
          66.0       2.7
          72.0       1.1
          73.0      12.0
          74.0      21.0
          75.0      75.5
          76.0      17.1
          77.0      75.2
          78.0     100.0
          79.0       8.2
          80.0       1.8
          84.0       3.2
          85.0       7.4
          86.0       5.6
          87.0       6.9
          88.0       2.7
          89.0      13.1
          90.0      35.2
          91.0       5.5
          92.0       1.1
          93.0       4.9
          94.0       9.3
          97.0       1.8
          98.0      18.5
          99.0      17.4
         100.0       7.8
         101.0       6.2
         104.0       1.2
         105.0       3.3
         106.0       4.7
         109.0       1.2
         110.0       8.9
         111.0      61.0
         112.0      17.7
         113.0      92.8
         114.0      12.9
         115.0      25.4
         116.0       2.8
         123.0       2.2
         124.0       8.6
         125.0      69.3
         126.0      15.6
         127.0      24.6
         128.0       5.6
         129.0       1.2
         134.0       1.5
         138.0       5.6
         139.0      24.3
         140.0       5.4
         141.0      14.6
         142.0       4.2
         143.0       3.0
         144.0       1.1
         153.0       2.4
         154.0       2.4
         155.0       3.0
         156.0       1.2
         157.0       1.0
         169.0       6.5
         170.0       1.8
         171.0       2.5
         187.0       1.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H6 Cl N O3 0.041 g : 0.5 ml CDCl3
    5-chloro-2-nitrobenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.070 B 7.806 C 7.425 D 5.010 E 2.58 J(A,C)=8.7HZ. J(B,C)=2.3HZ.

         Hz     ppm     Int.
    

        727.81   8.127    332
        719.06   8.029    442
        700.25   7.819    287
        698.06   7.795    312
        669.94   7.481    228
        667.56   7.454    197
        661.19   7.383    174
        658.88   7.357    152
        448.75   5.011   1000
        231.38   2.584    223
    

in CDCl3



KBr disc



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