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MassMS-IW-4171 D-lysine monohydrochloride C6H14N2O2 HCl (Mass of molecular ion: 146)
Source Temperature: 190 °C Sample Temperature: 180 °C Direct, 75 eV
15.0 1.1 17.0 2.1 18.0 14.2 27.0 3.9 28.0 22.3 29.0 7.2 30.0 79.0 31.0 3.1 35.0 5.2 36.0 66.1 37.0 1.8 38.0 22.2 39.0 3.3 41.0 11.4 42.0 12.9 43.0 23.0 44.0 17.1 45.0 4.7 46.0 1.9 53.0 1.5 54.0 3.9 55.0 12.8 56.0 71.0 57.0 14.8 58.0 3.5 59.0 8.4 65.0 1.1 67.0 10.0 68.0 2.1 69.0 4.8 70.0 9.7 71.0 10.9 72.0 87.6 73.0 9.4 74.0 20.1 75.0 5.2 81.0 1.0 82.0 9.5 83.0 12.2 84.0 100.0 85.0 9.2 87.0 2.6 88.0 3.1 89.0 3.0 99.0 2.2 100.0 10.0 101.0 6.3 110.0 2.1 111.0 3.3 112.0 1.6 117.0 3.7 128.0 6.0 129.0 14.0 130.0 7.2 146.0 1.0 147.0 4.4
400 MHz in D2O
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1H NMR 399.65 MHz C6 H14 N2 O2 0.040 g : 0.5 ml D2O D-lysine monohydrochloride 
Assign. Shift(ppm)
A 3.766 B 3.034 C 1.911 D 1.732 E 1.485 SOLVENT PEAK REMOVED
Hz ppm Int.1511.60 3.783 375 1505.37 3.767 727 1499.39 3.752 389 1220.46 3.054 764 1212.89 3.035 1000 1205.20 3.016 809 785.03 1.965 40 777.10 1.945 164 774.05 1.937 184 770.87 1.929 284 767.46 1.921 483 764.65 1.914 322 760.86 1.904 448 757.93 1.897 355 754.64 1.889 211 751.59 1.881 197 743.65 1.861 55 708.50 1.773 139 700.56 1.753 417 692.99 1.734 603 685.42 1.716 492 677.98 1.697 211 628.66 1.574 41 621.34 1.555 86 615.48 1.541 104 614.38 1.538 99 612.43 1.533 100 608.15 1.522 172 606.08 1.517 146 599.24 1.500 238 591.55 1.481 240 583.98 1.462 211 580.32 1.453 110 577.15 1.445 135 571.04 1.429 84 561.77 1.406 53
in D2O
KBr disc
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