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MS-NW-8049 phenyl 3-hydroxy-2-naphthoate C17H12O3 (Mass of molecular ion: 264)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 3.2 51.0 1.5 62.0 1.0 63.0 3.1 65.0 3.0 88.0 1.9 89.0 3.7 113.0 2.4 114.0 6.0 115.0 35.1 116.0 3.5 142.0 4.8 143.0 3.6 170.0 6.4 171.0 100.0 172.0 12.1 173.0 1.0 264.0 20.5 265.0 3.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C17 H12 O3 0.040 g : 0.5 ml CDCl3 phenyl 3-hydroxy-2-naphthoate Assign. Shift(ppm)
A 10.1 B 8.717 C 7.836 D 7.692 E 7.517 F 7.466 G 7.350 J 7.34 K 7.32 L 7.258
Hz ppm Int.
4056.40 10.150 1000 3484.19 8.719 677 3136.44 7.848 229 3135.68 7.847 246 3128.05 7.827 256 3127.29 7.826 267 3078.61 7.704 233 3070.98 7.685 286 3070.22 7.683 292 3012.39 7.538 171 3011.02 7.535 181 3005.52 7.521 218 3004.15 7.517 295 3002.78 7.514 155 2997.13 7.500 181 2995.91 7.497 178 2994.84 7.494 77 2992.55 7.488 291 2990.57 7.483 141 2987.52 7.476 73 2986.30 7.473 164 2985.08 7.470 532 2984.47 7.468 512 2982.03 7.462 108 2978.67 7.454 185 2976.84 7.449 469 2974.40 7.443 83 2941.13 7.360 211 2939.91 7.357 235 2937.62 7.351 692 2935.18 7.345 195 2933.96 7.342 419 2932.89 7.339 468 2931.67 7.336 233 2928.16 7.327 134 2926.48 7.323 427 2924.80 7.319 287 2920.23 7.307 102 2919.01 7.304 176 2917.94 7.302 109 2906.65 7.273 115 2905.27 7.270 549 2904.21 7.267 660 2901.92 7.262 177 2898.56 7.253 177 2897.80 7.251 282 2896.73 7.249 514 2895.51 7.246 472 2893.07 7.240 64
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