-
MassMS-NW-6159 (cyclopropylmethyl)amine hydrochloride C4H9N HCl (Mass of molecular ion: 71)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 5.5 16.0 1.1 17.0 17.5 18.0 82.8 26.0 2.3 27.0 12.6 28.0 22.6 29.0 9.2 30.0 100.0 31.0 1.6 35.0 2.6 36.0 13.7 37.0 1.7 38.0 4.3 39.0 13.3 40.0 2.6 41.0 9.2 42.0 26.8 43.0 89.8 44.0 3.4 45.0 2.7 46.0 2.8 47.0 6.8 50.0 7.2 51.0 1.8 52.0 2.3 53.0 5.0 54.0 5.9 55.0 12.5 56.0 5.8 61.0 2.5 62.0 7.9 67.0 1.1 68.0 2.2 70.0 13.3 71.0 17.3 82.0 1.3 84.0 9.3 124.0 1.1 125.0 1.6
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C4 H9 N 0.038 g : 0.5 ml DMSO-d6 (cyclopropylmethyl)amine hydrochloride 
Assign. Shift(ppm)
A 8.3 B 2.649 C 1.061 D 0.517 E 0.342
Hz ppm Int.3312.13 8.288 63 1062.62 2.659 990 1055.18 2.641 1000 439.58 1.100 44 436.65 1.093 60 434.94 1.089 37 431.88 1.081 123 428.83 1.074 108 427.49 1.070 88 424.19 1.062 198 421.02 1.054 90 419.43 1.050 114 416.26 1.042 130 413.33 1.035 37 411.62 1.030 70 408.69 1.023 42 224.24 0.562 47 222.29 0.557 49 218.14 0.546 39 215.82 0.541 193 211.43 0.530 462 209.59 0.525 485 207.76 0.520 227 205.32 0.514 247 203.25 0.509 483 201.42 0.504 399 197.27 0.494 196 143.80 0.360 200 139.53 0.350 540 137.94 0.346 466 134.89 0.338 437 133.30 0.334 526 128.66 0.322 128
in CDCl3
in DMSO-d6
KBr disc
nujol mull
更多供应商
