2，2-双（4-氯苯基）-1，1-二氯乙烯

产品名称 2，2-双（4-氯苯基）-1，1-二氯乙烯

CAS号72-55-9

分子式C14H8Cl4

分子量318.03

¹³CNMR

Mass

MS-NW-4606          
1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene
C14H8Cl4            (Mass of molecular ion:    316)

   Source Temperature: 270 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      36.0       1.1
      39.0       1.1
      50.0       4.1
      51.0       3.5
      61.0       1.4
      62.0       2.1
      63.0       2.2
      73.0       2.1
      74.0       5.5
      75.0       7.4
      76.0       1.1
      84.0       1.0
      85.0       1.7
      86.0       2.2
      87.0       5.6
      87.5       2.3
      88.0       4.1
      92.0       1.7
      93.0       1.2
      97.0       1.2
      98.0       2.8
      99.0       4.3
     100.0       1.0
     104.5       1.7
     105.0      12.2
     105.5       2.7
     106.0       4.2
     109.0       1.5
     110.0       2.9
     111.0       2.7
     122.0       5.5
     122.5       2.7
     123.0       8.9
     123.5       2.5
     124.0       4.1
     125.0       2.1
     126.0       1.1
     135.0       2.1
     136.0       1.3
     137.0       1.7
     140.0       5.4
     140.5       1.2
     141.0       5.6
     141.5       1.1
     142.0       1.9
     149.0       2.2
     150.0       3.3
     160.0       2.2
     162.0       1.0
     163.0       1.7
     170.0       4.0
     172.0       2.8
     173.0       1.3
     174.0       5.8
     175.0       7.6
     176.0      29.4
     177.0       4.5
     184.0       1.5
     185.0       1.1
     186.0       1.2
     199.0       1.5
     209.0       1.1
     210.0      14.3
     211.0       4.3
     212.0       5.3
     213.0       1.3
     233.0       2.9
     235.0       1.9
     244.0       1.3
     245.0       3.4
     246.0     100.0
     247.0      17.4
     248.0      63.7
     249.0      10.1
     250.0      10.9
     251.0       1.8
     280.0       5.8
     281.0       8.6
     282.0       6.7
     283.0       8.2
     284.0       3.0
     285.0       2.9
     316.0      56.5
     317.0       8.9
     318.0      68.4
     319.0      11.4
     320.0      34.9
     321.0       5.6
     322.0       7.7
     323.0       1.1

parameter in CDCl3

90 MHz in CDCl3

¹H NMR	300 MHz
C₁₄ H₈ Cl₄	ca 5 % in CDCl₃
1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene

    Parameter     ppm  Hz

      D(A)         7.24
      D(B)         7.12
       J(A,A')         2.1
       J(A,B)          8.4
       J(A,B')         0.5
       J(A',B)         0.5
       J(A',B')        8.4
       J(B,B')         2.1
     
     SHARPLESS,N.E. & BRADLEY,R.B. APPL.SPECTROSC. 22, 506 (1968)

     Hz     ppm     Int.

   2178.99   7.263     88
   2176.92   7.256    600
   2174.90   7.250    246
   2170.19   7.234    315
   2168.08   7.227   1000
   2166.09   7.220    171
   2141.91   7.140    171
   2139.93   7.133   1000
   2137.81   7.126    315
   2133.11   7.110    246
   2131.08   7.104    600
   2129.01   7.097     88

¹H NMR	89.56 MHz
C₁₄ H₈ Cl₄	0.045 g : 0.5 ml CDCl₃
1,1-dichloro-2,2-bis(p-chlorophenyl)ethylene

    Assign.     Shift(ppm)

      A             7.30
      B             7.21

     Hz     ppm     Int.

    666.63   7.444     27
    662.06   7.393     65
    660.69   7.378    206
    659.81   7.368    150
    658.06   7.348    111
    655.56   7.320     40
    654.31   7.306    160
    651.88   7.279   1000
    650.31   7.262    289
    648.81   7.245    357
    647.31   7.228    989
    644.81   7.200    178
    643.19   7.182     36
    642.50   7.174     36
    641.13   7.159    110
    639.31   7.139    152
    638.50   7.130    197
    637.06   7.114     52

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

更多供应商

2，2-双（4-氯苯基）-1，1-二氯乙烯(72-55-9)Raman光谱相关产品图谱

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