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MassMS-NW-1036 4-(aminomethyl)piperidine C6H14N2 (Mass of molecular ion: 114)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 2.3 17.0 1.3 18.0 6.4 26.0 1.2 27.0 9.4 28.0 21.5 29.0 14.0 30.0 84.3 31.0 2.3 39.0 7.9 40.0 1.5 41.0 15.3 42.0 24.3 43.0 21.0 44.0 10.0 51.0 1.3 52.0 1.4 53.0 4.5 54.0 7.2 55.0 37.9 56.0 100.0 57.0 41.6 58.0 13.9 67.0 7.7 68.0 11.7 69.0 31.4 70.0 10.6 71.0 3.1 79.0 1.5 80.0 3.5 81.0 2.9 82.0 17.4 83.0 2.5 84.0 38.8 85.0 28.9 86.0 12.5 94.0 1.4 96.0 17.7 97.0 14.4 98.0 2.1 114.0 28.3 115.0 2.2
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C6 H14 N2 0.05 ml : 0.5 ml CDCl3 4-(aminomethyl)piperidine 
Assign. Shift(ppm)
A 3.079 B 2.585 C 2.556 D 1.707 E 1.41 F 1.36 G 1.088 J(A,B)=-11.7HZ J(A,G)=4.2HZ J(B,D)=2.7HZ J(B,G)=12.2HZ J(C,E)=6.6HZ J(E,G)=J(D,G)=12.2HZ
Hz ppm Int.1240.60 3.105 159 1239.75 3.103 164 1236.57 3.095 263 1235.47 3.092 173 1233.40 3.087 176 1228.03 3.073 192 1227.42 3.072 190 1224.85 3.065 289 1221.92 3.058 181 1220.95 3.056 181 1047.49 2.622 262 1044.80 2.615 259 1041.50 2.607 37 1035.28 2.591 437 1032.59 2.584 429 1024.90 2.565 1000 1023.32 2.561 332 1020.51 2.554 295 1018.31 2.549 984 690.80 1.729 180 689.21 1.725 210 688.23 1.723 200 687.13 1.720 199 683.35 1.710 84 681.40 1.705 88 678.59 1.698 182 677.49 1.696 216 676.64 1.694 224 675.54 1.691 226 673.95 1.687 207 578.49 1.448 39 575.56 1.441 48 571.90 1.432 79 570.68 1.428 65 568.12 1.422 69 566.89 1.419 99 564.09 1.412 112 560.30 1.402 171 556.64 1.393 140 555.30 1.390 137 553.71 1.386 170 545.41 1.365 581 454.22 1.137 122 450.07 1.127 118 442.02 1.107 234 437.87 1.096 242 429.44 1.075 215 426.15 1.067 183 425.17 1.064 204 417.36 1.045 88 413.33 1.035 86
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1H NMR 89.56 MHz C6 H14 N2 0.04 ml : 0.5 ml CDCl3 4-(aminomethyl)piperidine Assign. Shift(ppm)
A 3.08 B 2.60 C 2.564 D 1.70 E 1.41 F 1.4 G 1.13
Hz ppm Int.282.44 3.154 72 273.94 3.059 75 273.44 3.054 69 273.06 3.049 68 272.56 3.044 71 271.00 3.026 102 270.00 3.015 104 268.25 2.996 79 267.25 2.985 63 244.44 2.730 86 242.06 2.703 73 232.13 2.592 460 226.38 2.528 347 220.88 2.467 68 160.13 1.788 62 159.81 1.785 64 159.00 1.776 59 158.38 1.769 61 150.75 1.684 65 149.56 1.670 58 148.25 1.656 72 147.06 1.643 84 146.63 1.638 81 145.50 1.625 69 144.81 1.617 61 126.00 1.407 1000 122.88 1.373 71 114.00 1.273 72 113.63 1.269 72 112.88 1.261 60 110.06 1.229 65 102.75 1.148 82 98.56 1.101 76
in CDCl3
CCl4 solution
liquid film
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