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MassMS-IW-9022 1-nitro-4-(trifluoromethoxy)benzene C7H4F3NO3 (Mass of molecular ion: 207)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.5 28.0 3.3 30.0 8.6 37.0 2.4 38.0 6.9 39.0 2.2 50.0 9.3 51.0 3.8 52.0 4.8 53.0 3.8 54.0 1.2 57.0 1.5 61.0 2.3 62.0 5.4 63.0 18.9 64.0 22.2 65.0 2.0 66.0 1.2 69.0 41.7 73.0 1.1 74.0 4.8 75.0 23.9 76.0 5.1 79.0 1.0 80.0 6.8 83.0 6.0 92.0 25.3 93.0 2.4 94.0 2.0 95.0 100.0 96.0 6.7 101.0 2.5 108.0 15.9 109.0 1.3 113.0 1.1 114.0 1.0 122.0 11.6 123.0 1.0 142.0 3.5 144.0 1.1 149.0 10.0 161.0 16.4 162.0 1.4 177.0 46.3 178.0 3.8 188.0 1.2 191.0 3.8 207.0 80.4 208.0 6.7 211.0 2.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H4 F3 N O3 0.05 ml : 0.5 ml CDCl3 1-nitro-4-(trifluoromethoxy)benzene 
Assign. Shift(ppm)
A 8.313 B 7.385
Hz ppm Int.3330.32 8.334 135 3327.15 8.326 980 3324.83 8.320 341 3320.07 8.308 364 3317.75 8.302 1000 3314.58 8.294 129 2959.47 7.406 77 2958.37 7.403 95 2956.30 7.398 470 2955.32 7.395 490 2954.22 7.393 293 2953.00 7.389 166 2952.03 7.387 85 2949.22 7.380 174 2948.12 7.377 293 2946.90 7.374 465 2945.92 7.372 431
in CDCl3
Liquid film
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