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MS-NW-1135 1-ethylimidazole C5H8N2 (Mass of molecular ion: 96)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.9 18.0 1.9 26.0 6.0 27.0 13.8 28.0 15.7 29.0 14.7 38.0 1.4 39.0 4.3 40.0 14.7 41.0 30.9 42.0 5.3 51.0 1.0 52.0 4.0 53.0 1.7 54.0 14.9 66.0 1.1 67.0 7.4 68.0 32.7 69.0 3.7 81.0 53.3 82.0 2.9 95.0 3.7 96.0 100.0 97.0 6.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H8 N2 0.05 ml : 0.5 ml CDCl3 1-ethylimidazole Assign. Shift(ppm)
A 7.45 B 7.018 C 6.913 D 3.952 E 1.408
Hz ppm Int.
667.50 7.454 177 629.63 7.031 157 628.56 7.019 264 627.56 7.008 183 623.81 6.966 24 620.44 6.928 196 619.19 6.914 297 617.94 6.900 153 365.50 4.082 115 358.13 3.999 359 350.81 3.918 382 343.50 3.836 140 133.38 1.490 509 126.13 1.409 1000 118.75 1.326 444
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