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网站主页CAS数据库列表 709-60-4更多图谱3-乙酰苯磺酰氯氟化物(709-60-4)质谱(MS)

3-乙酰苯磺酰氯氟化物

产品名称 3-乙酰苯磺酰氯氟化物

CAS号709-60-4

分子式C8H7FO3S

分子量202.2027832


  • Mass

    MS-NW-9956          
    m-acetylbenzenesulfonyl fluoride
    C8H7FO3S            (Mass of molecular ion:    202)
    

       Source Temperature: 230 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          15.0       1.6
          28.0       2.4
          39.0       1.3
          42.0       1.3
          43.0      26.8
          50.0       7.2
          51.0       2.4
          63.0       2.6
          64.0       3.2
          65.0       1.0
          74.0       3.0
          75.0       9.8
          76.0       7.4
          77.0       1.6
          83.0       2.2
          91.0       1.1
          92.0      22.5
          93.0       1.6
          95.0       3.7
         104.0       1.3
         159.0      15.5
         160.0       1.2
         187.0     100.0
         188.0       8.7
         189.0       5.4
         202.0       9.1
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H7 F O3 S 0.038 g : 0.5 ml DMSO-d6
    m-acetylbenzenesulfonyl fluoride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.52 B 8.51 C 8.405 D 7.982 E 2.719

         Hz     ppm     Int.
    

       3404.54   8.519    159
       3403.02   8.516    207
       3401.64   8.512     70
       3395.69   8.497     73
       3365.02   8.420     48
       3363.49   8.417     74
       3361.97   8.413     43
       3356.93   8.400     54
       3355.87   8.398     55
       3355.10   8.396     55
       3354.03   8.393     46
       3197.94   8.002     39
       3197.02   8.000     52
       3196.11   7.998     26
       3189.70   7.982     77
       3181.61   7.961     37
       3180.69   7.959     35
       1086.88   2.720   1000
       1083.53   2.712     23
    

in DMSO-d6



KBr disc



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