400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H13 O P 0.042 g : 0.5 ml CDCl3 3-methyl-1-phenyl-2-phospholene 1-oxide Assign. Shift(ppm)
A 7.69 B 7.49 C 5.945 D *1 2.83 E *1 2.63 F 2.23 G 2.083
Hz ppm Int.
3085.82 7.722 35 3084.11 7.718 49 3081.79 7.712 147 3080.44 7.708 187 3073.97 7.692 214 3072.27 7.688 216 3069.58 7.681 167 3068.24 7.678 200 3061.77 7.662 209 3060.18 7.658 191 3011.60 7.536 47 3010.25 7.533 58 3008.79 7.529 52 3007.57 7.526 47 3004.15 7.517 140 3002.81 7.514 151 2999.02 7.505 136 2997.44 7.501 244 2995.85 7.497 251 2993.41 7.491 289 2990.72 7.484 274 2985.60 7.471 275 2983.52 7.466 257 2979.61 7.456 97 2977.42 7.451 97 2974.85 7.444 57 2389.40 5.979 134 2388.18 5.976 135 2364.38 5.917 135 2363.04 5.913 134 1147.71 2.872 42 1146.97 2.870 41 1142.58 2.859 47 1142.21 2.859 47 1137.82 2.848 55 1134.64 2.840 44 1130.37 2.829 72 1124.51 2.814 66 1116.58 2.794 34 1116.21 2.793 34 1064.82 2.665 49 1063.84 2.662 46 1062.74 2.660 45 1061.89 2.658 44 1059.08 2.651 58 1058.35 2.649 59 1057.74 2.647 60 1057.50 2.647 60 1054.93 2.640 54 1054.32 2.639 54 1053.34 2.636 56 1052.86 2.635 55 1051.76 2.632 54 1047.85 2.622 56 1047.49 2.622 55 1042.97 2.610 36 1040.89 2.605 39 1040.65 2.604 39 1039.92 2.603 39 907.71 2.272 69 903.08 2.260 74 898.44 2.249 109 893.68 2.237 133 891.97 2.232 121 889.40 2.226 148 886.47 2.219 119 884.28 2.213 196 881.23 2.206 102 878.42 2.198 91 876.22 2.193 78 873.90 2.187 37 832.76 2.084 1000
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