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MassMS-NW-6423 trimethyl orthobenzoate C10H14O3 (Mass of molecular ion: 182)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 6.4 29.0 1.9 31.0 1.2 39.0 1.2 45.0 2.0 50.0 3.5 51.0 9.4 59.0 10.5 65.0 1.4 74.0 1.0 75.0 1.1 76.0 1.4 77.0 23.9 78.0 2.1 79.0 1.3 91.0 11.3 92.0 3.3 105.0 47.0 106.0 3.8 136.0 3.6 151.0 100.0 152.0 10.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H14 O3 0.05 ml : 0.5 ml CDCl3 trimethyl orthobenzoate 
Assign. Shift(ppm)
A 7.55 B 7.42 to 7.29 C 3.128
Hz ppm Int.683.88 7.637 20 679.94 7.593 34 678.94 7.581 25 676.38 7.553 46 674.00 7.526 55 664.38 7.419 31 663.50 7.409 26 661.94 7.392 66 660.81 7.379 56 657.56 7.343 64 654.88 7.313 58 280.25 3.130 1000
in CDCl3
liquid film
4880 A,200 M,liquid
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