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MS-NW-7499 (bromomethyl)cyclopropane C4H7Br (Mass of molecular ion: 134)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
26.0 4.5 27.0 22.5 28.0 5.3 29.0 22.6 37.0 1.1 38.0 1.8 39.0 13.9 40.0 1.0 41.0 5.4 44.0 1.4 50.0 2.1 51.0 2.3 53.0 6.2 54.0 2.5 55.0 100.0 56.0 4.6 106.0 6.8 108.0 6.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H7 Br 0.05 ml : 0.5 ml CDCl3 (bromomethyl)cyclopropane Assign. Shift(ppm)
A 3.334 B 1.301 C 0.757 D 0.359
Hz ppm Int.
1336.30 3.344 969 1328.74 3.325 1000 536.01 1.342 61 533.08 1.334 86 528.32 1.322 162 525.15 1.315 126 523.56 1.311 103 520.39 1.303 241 517.33 1.295 105 515.63 1.291 132 512.57 1.283 181 507.81 1.271 102 504.88 1.264 65 311.89 0.781 146 307.25 0.769 393 305.91 0.766 436 304.93 0.763 284 301.39 0.755 170 300.90 0.753 183 299.32 0.749 418 297.97 0.746 369 297.12 0.744 284 292.97 0.734 155 152.10 0.381 166 147.46 0.369 465 146.24 0.366 410 143.68 0.360 219 142.70 0.358 389 141.36 0.354 488 136.84 0.343 116 136.11 0.341 118
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