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MassMS-NW-3499 2,5-dimethyl-1-hexene C8H16 (Mass of molecular ion: 112)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.1 27.0 11.8 28.0 1.7 29.0 15.4 38.0 1.2 39.0 15.9 40.0 3.0 41.0 46.4 42.0 5.3 43.0 11.3 50.0 1.0 51.0 1.8 53.0 5.6 54.0 2.0 55.0 31.1 56.0 100.0 57.0 40.4 58.0 1.9 67.0 2.7 68.0 2.1 69.0 15.5 70.0 3.7 81.0 1.0 97.0 1.4 112.0 10.5 113.0 1.1
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C8 H16 0.04 ml : 0.5 ml CDCl3 2,5-dimethyl-1-hexene 
Assign. Shift(ppm)
A 4.67 B 2.00 C 1.712 D 1.57 E 1.33 F 0.897
Hz ppm Int.419.75 4.687 153 418.63 4.675 273 417.63 4.664 281 416.50 4.651 155 187.63 2.096 57 180.63 2.017 83 177.63 1.984 51 172.38 1.925 94 154.50 1.726 344 153.44 1.714 557 152.19 1.700 353 145.88 1.629 30 140.38 1.568 39 139.19 1.555 45 133.00 1.486 42 128.25 1.433 88 127.00 1.419 98 125.31 1.400 49 123.69 1.382 43 122.19 1.365 82 120.81 1.349 49 119.38 1.333 113 118.63 1.325 84 117.00 1.307 60 114.19 1.276 43 112.25 1.254 116 110.88 1.239 39 106.63 1.191 39 104.75 1.170 31 82.94 0.927 1000 76.94 0.860 775
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1H NMR 399.65 MHz C8 H16 0.05 ml : 0.5 ml CDCl3 2,5-dimethyl-1-hexene Assign. Shift(ppm)
A 4.67 B 2.006 C 1.715 D 1.536 E 1.317 F 0.894
Hz ppm Int.1872.44 4.686 46 1871.70 4.684 55 1870.85 4.682 73 1870.12 4.680 86 1869.38 4.678 82 1868.65 4.676 85 1867.80 4.674 70 1866.21 4.670 89 1865.36 4.668 92 1864.01 4.665 69 1863.04 4.662 47 809.33 2.026 58 801.88 2.007 68 793.46 1.986 61 686.40 1.718 277 685.55 1.716 345 621.34 1.555 46 614.62 1.538 58 608.03 1.522 50 536.50 1.343 79 531.62 1.331 33 530.40 1.328 57 529.66 1.326 105 528.20 1.322 97 526.49 1.318 47 525.27 1.315 34 524.78 1.314 34 523.56 1.311 40 521.85 1.306 61 521.12 1.304 69 520.26 1.302 112 513.67 1.286 55 366.46 0.917 30 360.72 0.903 1000 354.00 0.886 888
in CDCl3
liquid film
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