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MassMS-KW-0514 4-bromophthalimide C8H4BrNO2 (Mass of molecular ion: 225)
Source Temperature: 130 °C Sample Temperature: 130 °C Direct, 75 eV
28.0 4.9 37.0 8.9 37.5 2.6 38.0 4.1 44.0 1.1 44.5 2.8 45.0 1.3 49.0 3.1 50.0 6.8 50.5 1.3 51.0 4.0 52.0 1.2 53.0 1.6 59.0 2.2 61.0 2.5 62.0 3.1 63.0 3.7 70.0 1.9 72.0 1.1 73.0 10.8 74.0 43.1 75.0 77.2 76.0 5.7 77.0 7.6 78.0 6.2 84.5 4.2 85.5 4.1 90.0 1.0 91.0 2.0 92.0 1.7 98.5 2.0 99.5 2.6 100.0 1.2 101.0 1.2 102.0 11.6 103.0 9.6 104.0 1.1 106.0 1.0 153.0 2.0 154.0 42.6 155.0 4.8 156.0 41.6 157.0 3.0 168.0 2.2 170.0 3.0 181.0 24.6 182.0 53.2 183.0 27.9 184.0 51.7 185.0 4.0 225.0 100.0 226.0 9.5 227.0 98.0 228.0 9.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C8H4BrNO2 0.039 g : 0.5 ml DMSO-d6 4-bromophthalimide 
Assign. Shift(ppm)
A 11.5 B 8.014 C 7.980 D 7.757
Hz ppm Int.4594.68 11.493 98 3208.75 8.027 437 3207.10 8.023 562 3200.87 8.007 487 3199.22 8.003 690 3190.98 7.982 1000 3189.88 7.980 712 3189.33 7.978 763 3104.33 7.766 842 3096.46 7.746 711
in DMSO-d6
KBr disk
Nujol
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