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1-甲基-1,2,3,6-四氢吡啶

产品名称 1-甲基-1,2,3,6-四氢吡啶

CAS号694-55-3

分子式C6H11N

分子量97.16

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  • Mass

    MS-NW-6409          
    1-methyl-1,2,3,6-tetrahydropyridine
    C6H11N              (Mass of molecular ion:     97)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       9.4
          17.0       1.1
          18.0       5.1
          26.0       2.7
          27.0      12.9
          28.0       7.2
          29.0       3.0
          30.0       3.4
          37.0       1.1
          38.0       2.3
          39.0      20.4
          40.0       2.9
          41.0      14.1
          42.0     100.0
          43.0      55.1
          44.0      19.2
          45.0       3.3
          50.0       2.3
          51.0       3.9
          52.0       4.1
          53.0       9.8
          54.0      42.1
          55.0       8.7
          56.0       2.3
          57.0       1.5
          65.0       2.0
          66.0       1.5
          67.0       6.1
          68.0      17.7
          69.0       4.6
          70.0       2.4
          78.0       1.5
          79.0       3.3
          80.0       5.9
          81.0       9.7
          82.0      23.5
          83.0       1.7
          91.0       1.2
          92.0       1.3
          93.0       1.1
          94.0      18.2
          95.0       2.5
          96.0      86.5
          97.0      92.4
          98.0       7.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H11 N 0.05 ml : 0.5 ml CDCl3
    1-methyl-1,2,3,6-tetrahydropyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.729 B 5.659 C 2.904 D 2.503 E 2.334 F 2.19

         Hz     ppm     Int.
    

       1166.50   2.919     89
       1163.45   2.912    211
       1161.38   2.906    221
       1160.52   2.904    241
       1158.45   2.899    213
       1155.52   2.892     89
       1006.35   2.519    220
       1000.61   2.504    412
        994.87   2.490    255
        935.79   2.342    103
        932.98   2.335   1000
        886.23   2.218     31
        883.42   2.211     62
        881.47   2.206     74
        880.62   2.204     94
        877.81   2.197    128
        875.73   2.192    119
        875.12   2.190    127
        874.27   2.188    118
        872.31   2.183    126
        869.38   2.176     88
        866.58   2.169     54
    

in CDCl3



liquid film