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网站主页CAS数据库列表 693-02-7更多图谱1-己炔(693-02-7)核磁图(1HNMR)

1-己炔

产品名称 1-己炔

CAS号693-02-7

分子式C6H10

分子量82.14

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  • Mass

    MS-NW-1217          
    1-hexyne
    C6H10               (Mass of molecular ion:     82)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       1.4
          18.0       2.3
          26.0       3.3
          27.0      44.1
          28.0       4.8
          29.0       5.8
          37.0       2.4
          38.0       5.7
          39.0      36.2
          40.0      24.6
          41.0      64.3
          42.0      15.9
          43.0      48.9
          44.0       1.7
          50.0       5.8
          51.0       8.0
          52.0       4.2
          53.0      15.4
          54.0      27.0
          55.0       3.4
          56.0       4.5
          63.0       1.5
          65.0       4.5
          66.0       1.7
          67.0     100.0
          68.0       6.2
          77.0       1.8
          79.0       2.8
          81.0      10.9
          97.0       3.8
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H10 0.02 ml : 0.5 ml CDCl3
    1-hexyne
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.18 B 1.931 C 1.52 D 1.41 E 0.92

         Hz     ppm     Int.
    

        204.25   2.281     81
        202.75   2.264    114
        201.56   2.251    116
        200.31   2.237    126
        199.50   2.228     99
        197.56   2.206    399
        195.00   2.178    436
        193.56   2.162    145
        192.63   2.151    118
        191.44   2.138    167
        190.56   2.128    183
        188.63   2.107    205
        175.31   1.958    650
        172.81   1.930    829
        170.06   1.899    426
        143.94   1.608     88
        143.19   1.599     79
        142.50   1.592     88
        140.81   1.573    210
        137.56   1.536    298
        135.38   1.512    253
        133.69   1.493    573
        131.06   1.464    343
        130.06   1.453    464
        129.25   1.444    276
        128.06   1.430    255
        127.56   1.425    260
        127.44   1.423    260
        126.50   1.413    376
        124.50   1.391    194
        122.56   1.369    152
        119.50   1.335    102
        116.38   1.300     91
         89.56   1.000    213
         88.75   0.991    375
         88.13   0.985    301
         86.56   0.967    171
         85.50   0.955    208
         85.38   0.954    208
         83.81   0.936    198
         82.19   0.918   1000
         79.25   0.885    271
         77.50   0.866    158
         75.94   0.848    153
         74.75   0.835    166
         73.13   0.817    104
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid