图谱信息 供应商 相关产品
网站主页CAS数据库列表 68494-08-6更多图谱4,5-双(苄基硫代)-1,3-二硫杂环戊二烯-2-噻酮(68494-08-6)核磁图(1HNMR)

4,5-双(苄基硫代)-1,3-二硫杂环戊二烯-2-噻酮

产品名称 4,5-双(苄基硫代)-1,3-二硫杂环戊二烯-2-噻酮

CAS号68494-08-6

分子式C17H10O2S5

分子量406.59

展开


  • Mass

    MS-NW-7003          
    4,5-bis(benzoylthio)-1,3-dithiole-2-thione
    C17H10O2S5          (Mass of molecular ion:    406)
    

       Source Temperature: 200 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          17.0       1.4
          18.0       5.6
          50.0       2.1
          51.0       8.2
          76.0       3.8
          77.0      32.7
          78.0       2.5
         105.0     100.0
         106.0       8.4
         406.0       4.3
         407.0       1.0
         408.0       1.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C17 H10 O2 S5 0.040 g : 0.5 ml CDCl3
    4,5-bis(benzoylthio)-1,3-dithiole-2-thione
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.94 B 7.67 C 7.51

         Hz     ppm     Int.
    

        718.88   8.027     87
        716.31   7.999    540
        714.88   7.983    665
        713.13   7.963    349
        710.63   7.935    289
        708.50   7.911    880
        706.63   7.891    893
        701.88   7.837     64
        695.94   7.771     83
        694.38   7.754    134
        692.81   7.736    116
        691.25   7.719     97
        690.06   7.706     63
        689.63   7.701     70
        686.81   7.669    375
        684.13   7.639    196
        682.00   7.616    424
        680.31   7.597    690
        678.06   7.572    892
        677.38   7.564   1000
        675.94   7.548    442
        672.75   7.512    361
        671.63   7.500    393
        670.19   7.484    776
        668.00   7.459    205
        666.38   7.441    116
        665.31   7.429    170
        663.75   7.412    250
        661.38   7.385    185
    

KBr disc



nujol mull