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MassMS-IW-2197 6-bromo-4-methyl-1-phenylnaphtho(1,2,3-de)quinoline-2,7(3H)-dione C23H14BrNO2 (Mass of molecular ion: 415)
Source Temperature: 190 °C Sample Temperature: 180 °C Direct, 75 eV
51.0 1.1 63.0 1.0 75.0 1.3 77.0 1.2 80.0 1.6 82.0 1.6 87.0 1.7 99.0 1.6 100.0 2.7 105.5 1.1 106.0 1.0 111.0 1.5 111.5 1.4 112.0 5.8 112.5 2.8 113.0 5.4 113.5 1.3 117.5 1.3 118.0 1.8 118.5 2.8 119.0 1.4 119.5 1.3 124.0 3.6 124.5 2.9 125.0 11.4 125.5 4.7 126.0 8.3 126.5 2.4 127.0 1.0 130.0 1.2 130.5 4.7 131.0 4.7 131.5 7.4 132.0 3.2 132.5 2.5 137.5 1.5 138.0 4.2 138.5 5.2 139.0 10.9 139.5 4.7 140.0 1.5 143.5 1.4 144.0 3.8 144.5 15.3 145.0 6.8 145.5 2.4 146.0 1.1 150.0 2.0 151.0 2.3 152.5 1.6 153.0 1.7 153.5 8.7 154.0 4.9 154.5 1.0 158.5 1.9 159.0 7.7 159.5 2.3 167.5 1.1 168.0 1.4 174.0 1.3 175.0 1.8 176.0 6.6 177.0 3.6 184.5 1.2 185.5 1.9 186.0 1.0 187.0 1.0 198.0 1.2 198.5 3.6 199.0 2.1 199.5 3.7 200.0 2.1 201.0 1.4 202.0 1.2 205.0 1.3 207.5 7.5 208.0 2.1 208.5 7.7 209.0 2.0 213.0 1.1 224.0 2.3 225.0 1.9 226.0 2.1 227.0 1.2 237.0 1.7 238.0 1.8 239.0 1.2 248.0 1.4 249.0 1.8 250.0 6.2 251.0 4.4 252.0 6.4 253.0 2.7 261.0 1.6 262.0 2.6 263.0 3.8 264.0 5.8 265.0 2.9 275.0 2.9 276.0 3.1 277.0 10.5 278.0 15.1 279.0 6.9 280.0 4.4 281.0 1.2 288.0 7.1 289.0 9.6 290.0 6.6 291.0 1.8 293.0 1.1 306.0 11.0 307.0 9.7 308.0 4.2 309.0 1.2 316.0 1.4 317.0 5.6 318.0 5.4 319.0 2.1 324.0 1.1 334.0 5.8 335.0 46.7 336.0 24.8 337.0 11.7 338.0 2.5 368.0 8.7 369.0 2.5 370.0 16.1 371.0 10.7 372.0 5.0 373.0 3.2 386.0 3.4 387.0 3.8 388.0 4.8 389.0 3.4 390.0 1.7 396.0 6.6 397.0 4.3 398.0 8.8 399.0 4.6 400.0 3.1 414.0 76.9 415.0 100.0 416.0 97.8 417.0 99.2 418.0 22.9 419.0 3.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C23 H14 Br N O2 saturated in DMSO-d6 6-bromo-4-methyl-1-phenylnaphtho(1,2,3-de)quinoline-2,7(3H)-dione 
Assign. Shift(ppm)
A 11.4 B 8.101 C 7.870 D 7.49 E 7.45 F 7.38 G 7.215 J 7.040 K 2.602
Hz ppm Int.4540.33 11.361 37 3242.41 8.114 158 3241.31 8.111 163 3234.72 8.094 175 3233.62 8.092 168 3145.88 7.872 324 3145.34 7.871 327 3001.37 7.510 119 3000.45 7.508 124 2998.80 7.504 51 2996.60 7.499 55 2993.31 7.490 219 2988.73 7.479 79 2988.36 7.478 82 2986.35 7.473 177 2985.25 7.470 170 2983.97 7.467 117 2980.12 7.457 406 2977.01 7.450 476 2975.91 7.447 372 2973.52 7.441 490 2971.69 7.436 230 2967.11 7.425 64 2966.02 7.422 58 2965.47 7.421 56 2964.92 7.419 58 2964.00 7.417 55 2963.45 7.416 57 2963.08 7.415 56 2962.35 7.413 53 2961.99 7.412 52 2961.62 7.411 52 2961.07 7.410 55 2960.52 7.408 58 2957.77 7.401 93 2956.49 7.398 120 2954.29 7.393 319 2952.83 7.389 241 2951.73 7.386 308 2949.90 7.382 226 2948.06 7.377 255 2946.97 7.374 173 2946.42 7.373 169 2944.77 7.369 186 2941.47 7.361 52 2892.20 7.237 105 2890.73 7.234 104 2884.87 7.219 125 2883.77 7.216 171 2882.49 7.213 143 2876.63 7.198 112 2875.16 7.195 111 2817.47 7.050 199 2817.10 7.049 202 2809.22 7.030 165 2808.86 7.029 164 1040.02 2.603 1000
KBr disc
nujol mull
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