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MassMS-IW-1780 3-chloro-2,6-diethylaniline C10H14ClN (Mass of molecular ion: 183)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 1.3 28.0 1.1 39.0 2.5 41.0 1.1 51.0 3.3 52.0 1.7 53.0 1.3 58.5 1.9 63.0 2.1 64.5 1.8 65.0 3.7 65.5 1.7 66.0 1.0 75.0 1.4 76.5 6.2 77.0 5.5 77.5 2.0 78.0 1.6 83.5 1.0 89.0 1.9 90.0 1.1 91.0 5.2 102.0 1.5 103.0 2.2 104.0 1.7 105.0 1.9 115.0 4.1 116.0 2.7 117.0 6.6 118.0 3.6 119.0 2.7 120.0 1.0 127.0 1.3 128.0 1.9 129.0 1.0 130.0 3.8 131.0 3.4 132.0 4.9 133.0 10.6 134.0 1.1 140.0 1.5 148.0 2.6 151.0 1.4 152.0 1.6 153.0 5.6 154.0 2.8 155.0 2.0 166.0 1.9 168.0 100.0 169.0 10.5 170.0 31.8 171.0 3.3 182.0 2.2 183.0 39.8 184.0 5.3 185.0 13.0 186.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 Cl N 0.05 ml : 0.5 ml CDCl3 3-chloro-2,6-diethylaniline 
Assign. Shift(ppm)
A 6.816 B 6.752 C 3.68 D 2.705 E 2.425 F 1.203 G 1.142
Hz ppm Int.2729.25 6.830 184 2721.07 6.809 312 2701.42 6.760 363 2693.24 6.739 216 1474.37 3.690 55 1092.53 2.734 146 1084.84 2.715 418 1077.27 2.696 423 1069.70 2.677 152 980.59 2.454 116 973.14 2.435 326 965.58 2.417 332 957.89 2.397 124 488.16 1.222 605 485.84 1.216 34 480.59 1.203 1000 478.27 1.197 61 473.02 1.184 568 470.83 1.179 39 464.11 1.162 533 456.54 1.143 941 448.85 1.124 513
in CDCl3
liquid film
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