400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H18 O Si2 20 mg : 0.5 ml CDCl3 1,3-dimethyl-1,3-diphenyldisiloxane Assign. Shift(ppm)
A 7.557 B 7.39 C 7.362 D 5.148 E 0.428
Hz ppm Int.
3027.47 7.576 37 3025.51 7.571 164 3024.66 7.569 210 3023.93 7.567 239 3023.07 7.565 253 3022.09 7.562 162 3020.02 7.557 100 3019.04 7.555 135 3018.07 7.552 242 3017.09 7.550 257 3016.11 7.547 271 3015.26 7.545 237 2963.50 7.416 36 2956.18 7.397 149 2953.13 7.390 65 2951.17 7.385 140 2949.71 7.381 233 2949.34 7.380 238 2947.27 7.375 353 2939.58 7.356 287 2933.35 7.340 85 2931.27 7.335 62 2062.01 5.160 61 2061.28 5.158 71 2059.20 5.153 167 2058.47 5.151 181 2056.40 5.146 170 2055.54 5.144 177 2053.59 5.139 66 2052.73 5.137 65 176.15 0.441 69 172.73 0.433 1000 169.92 0.426 963 166.26 0.417 59
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