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网站主页CAS数据库列表 66750-10-5更多图谱苯杂氮-15-冠-5(66750-10-5)红外图谱(IR2)

苯杂氮-15-冠-5

产品名称 苯杂氮-15-冠-5

CAS号66750-10-5

分子式C16H25NO4

分子量295.37

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  • Mass

    MS-IW-5012          
    13-phenyl-1,4,7,10-tetraoxa-13-azacyclopentadecane
    C16H25NO4           (Mass of molecular ion:    295)
    

       Source Temperature: 160 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          15.0       1.2
          27.0       1.7
          28.0       2.8
          29.0       1.8
          31.0       2.5
          41.0       1.5
          42.0       2.1
          43.0       5.8
          44.0       2.7
          45.0      10.3
          51.0       2.4
          56.0       1.5
          59.0       1.5
          65.0       1.4
          71.0       1.2
          73.0       1.1
          77.0      15.3
          78.0       2.1
          79.0       1.5
          86.0       1.4
          87.0       2.3
          88.0       1.0
          88.5       1.8
          89.0       1.3
          91.0      19.5
          92.0       2.2
          93.0       8.0
          95.5       1.6
         100.0       1.3
         103.0       1.1
         104.0      14.7
         105.0      27.1
         106.0      41.7
         107.0       3.8
         110.5       1.4
         117.0       2.7
         118.0       5.8
         119.0      31.7
         120.0      21.5
         121.0       3.2
         130.0       2.3
         131.0       2.4
         132.0      16.9
         133.0       7.1
         134.0       5.8
         135.0       1.5
         137.0      12.8
         138.0       1.4
         144.0       4.5
         145.0       1.3
         146.0      15.7
         147.0       7.2
         148.0      11.8
         149.0      17.0
         150.0      25.1
         151.0       5.1
         158.0       1.1
         162.0      26.5
         163.0      12.8
         164.0      11.9
         165.0       1.7
         176.0      17.7
         177.0       9.2
         178.0       4.5
         179.0       3.8
         181.0       1.0
         188.0       2.1
         190.0       4.5
         192.0       3.4
         194.0       1.5
         206.0       2.0
         207.0       4.2
         208.0       8.1
         209.0       2.6
         220.0       5.8
         221.0       1.3
         234.0       3.3
         236.0       3.1
         237.0       1.9
         238.0       3.9
         239.0       5.7
         250.0       1.9
         252.0       1.1
         264.0      10.0
         265.0       4.6
         267.0       8.1
         268.0       1.3
         294.0       2.1
         295.0     100.0
         296.0      19.0
         297.0       2.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H25 N O4 0.038 g : 0.5 ml CDCl3
    13-phenyl-1,4,7,10-tetraoxa-13-azacyclopentadecane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.202 B 6.66 C 6.65 D 3.750 E 3.667 F 3.646 G 3.633 J 3.593

         Hz     ppm     Int.
    

       2886.84   7.224     74
       2879.39   7.205     87
       2878.66   7.203     78
       2877.81   7.201     78
       2870.61   7.183     88
       2665.77   6.671     64
       2664.67   6.668    107
       2661.87   6.661     41
       2660.28   6.657     41
       2659.18   6.654     94
       2658.08   6.652     67
       2655.88   6.646     83
       2655.03   6.644     93
       2652.83   6.638     40
       2651.86   6.636     39
       1505.74   3.768    106
       1499.51   3.753    288
       1493.41   3.737    159
       1472.17   3.684     59
       1470.70   3.680     76
       1468.99   3.676    119
       1466.92   3.671    108
       1465.33   3.667    150
       1463.87   3.663    257
       1463.26   3.662    262
       1458.74   3.651    244
       1458.13   3.649    272
       1456.79   3.646    168
       1455.08   3.641    133
       1452.03   3.634   1000
       1441.41   3.607    161
       1435.30   3.592    262
       1428.96   3.576    105
    

in CDCl3



KBr disc



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