N,N’-1,3-亚丙基二[2-(乙烯基磺酰基)]乙酰胺

产品名称 N,N’-1,3-亚丙基二[2-(乙烯基磺酰基)]乙酰胺

CAS号66710-66-5

分子式C10H16N2O6S2

分子量324.37

¹³CNMR

Mass

MS-IW-8112          
N,N'-ethylenebis((vinylsulfonyl)acetamide)
C10H16N2O6S2        (Mass of molecular ion:    324)

   Source Temperature: 160 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      15.0       1.9
      17.0       3.1
      18.0      16.4
      25.0       1.0
      26.0       6.9
      27.0      20.1
      28.0      11.8
      29.0       2.7
      30.0      73.8
      31.0       1.8
      34.0       1.3
      36.0       3.1
      38.0       1.3
      39.0       2.6
      40.0       2.5
      41.0       8.6
      42.0      11.0
      43.0      20.1
      44.0       9.8
      45.0       2.8
      46.0       1.0
      47.0       1.3
      48.0       6.4
      52.0       1.0
      53.0       1.3
      54.0       6.7
      55.0       5.3
      56.0       4.5
      57.0       2.4
      58.0       2.6
      59.0       3.1
      60.0       2.6
      63.0       3.4
      64.0      19.2
      65.0       2.2
      66.0       1.8
      67.0       1.2
      68.0       2.3
      69.0       2.8
      70.0       1.6
      71.0       4.3
      72.0     100.0
      73.0       6.4
      75.0       2.0
      76.0       2.3
      81.0       2.8
      82.0       2.8
      83.0      17.7
      84.0      56.6
      85.0       9.9
      86.0       3.2
      87.0       5.7
      89.0       1.0
      91.0      20.4
      93.0       2.2
      98.0       2.4
      99.0       2.1
     100.0       2.6
     101.0       2.6
     109.0       1.8
     110.0       1.3
     111.0       2.8
     117.0       1.1
     120.0       1.9
     132.0       1.0
     133.0       5.9
     150.0       4.1
     162.0      16.6
     163.0       6.0
     164.0       1.3
     173.0       5.4
     174.0       2.1
     175.0      35.0
     176.0       5.6
     177.0       2.2
     191.0      37.1
     192.0       3.2
     193.0       2.4
     204.0       4.9
     215.0       1.2
     233.0      26.8
     234.0       3.1
     235.0       1.8
     325.0       4.9

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₆ N₂ O₆ S₂	0.039 g : 0.5 ml DMSO-d₆
N,N'-ethylenebis((vinylsulfonyl)acetamide)

    Assign.     Shift(ppm)

      A             8.35
      B             7.024
      C             6.257
      D             6.244
      E             4.082
      F             3.152

     Hz     ppm     Int.

   3337.40   8.351    117
   2821.04   7.059    200
   2811.04   7.034    225
   2804.44   7.018    238
   2794.43   6.993    233
   2505.00   6.268    410
   2503.17   6.264    384
   2495.12   6.244    351
   2486.57   6.222    316
   1631.84   4.084   1000
   1267.94   3.173     76
   1262.57   3.160    294
   1259.89   3.153    259
   1257.32   3.147    281

in DMSO-d6

KBr disc

nujol mull

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