5-氯-2-硝基苯甲醛

Mass

MS-NW-0209          
5-chloro-2-nitrobenzaldehyde
C7H4ClNO3           (Mass of molecular ion:    185)

   Source Temperature: 160 °C
   Sample Temperature:   0 °C
   Direct, 75 eV

      27.0       1.1
      29.0       5.9
      30.0      10.7
      37.0       5.6
      38.0       5.2
      39.0       4.2
      49.0       3.3
      50.0      29.0
      51.0      12.5
      52.0       1.4
      53.0       3.4
      60.0       1.5
      61.0       4.9
      62.0       4.9
      63.0      14.8
      64.0       2.8
      72.0       1.1
      73.0      23.7
      74.0      34.9
      75.0      86.5
      76.0      13.8
      77.0       1.8
      78.0      10.0
      84.0       5.6
      85.0       8.9
      86.0       2.5
      87.0       3.1
      88.0       1.0
      90.0       2.0
      91.0       1.3
      92.0       1.3
      98.0       2.3
      99.0      88.0
     100.0       5.5
     101.0      28.0
     102.0       1.7
     109.0       2.5
     110.0      38.4
     111.0      16.5
     112.0      14.5
     113.0       7.3
     124.0       1.4
     125.0       1.6
     126.0       2.3
     127.0      85.6
     128.0       6.7
     129.0      28.6
     130.0       1.8
     138.0      29.0
     139.0       2.7
     140.0       9.6
     141.0       3.3
     155.0     100.0
     156.0       8.0
     157.0      32.0
     158.0       2.5
     168.0       3.1
     170.0       1.0
     185.0       9.7
     186.0       1.3
     187.0       3.1

Assign. Shift(ppm) A 10.412 B 8.113 C 7.890 D 7.726 J(B,D)=8.6HZ. J(C,D)=2.4HZ.

     Hz     ppm     Int.

    932.59  10.414   1000
    732.13   8.175    201
    723.49   8.079    322
    708.25   7.909    270
    707.89   7.905    294
    705.91   7.882    406
    705.54   7.878    347
    696.39   7.776    355
    693.97   7.749    247
    687.74   7.680    217
    685.40   7.653    172