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网站主页CAS数据库列表 6628-06-4更多图谱2-烯丙基-4-甲基苯酚(6628-06-4)核磁图(13CNMR)

2-烯丙基-4-甲基苯酚

产品名称 2-烯丙基-4-甲基苯酚

CAS号6628-06-4

分子式C10H12O

分子量148.2

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  • Mass

    MS-NW-5755          
    2-allyl-4-methylphenol
    C10H12O             (Mass of molecular ion:    148)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       5.3
          38.0       1.2
          39.0       8.4
          40.0       1.3
          41.0       4.8
          43.0       1.8
          50.0       2.6
          51.0       7.9
          52.0       3.3
          53.0       4.0
          55.0       4.3
          62.0       1.3
          63.0       3.8
          64.0       3.2
          65.0       5.9
          66.0       1.7
          72.0       1.5
          73.0       2.1
          74.0       1.1
          75.0       1.0
          77.0      14.3
          78.0       5.3
          79.0       5.3
          89.0       1.7
          91.0      16.1
          92.0       4.9
          93.0       2.3
         102.0       1.3
         103.0       5.3
         104.0       2.7
         105.0      29.7
         106.0       3.1
         107.0       7.4
         108.0       1.2
         115.0      11.3
         116.0       2.5
         117.0       2.1
         119.0       6.3
         120.0       3.7
         121.0      11.1
         122.0       1.2
         127.0       1.8
         128.0       3.4
         129.0       5.3
         130.0       1.3
         131.0       8.2
         132.0       5.2
         133.0      56.7
         134.0       5.6
         145.0       2.7
         146.0       1.4
         147.0      15.6
         148.0     100.0
         149.0      11.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H12 O 0.04 ml : 0.5 ml CDCl3
    2-allyl-4-methylphenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.90 B 6.90 C 6.690 D 5.981 E 5.13 F 5.13 G 4.8 J 3.358 K 2.245

         Hz     ppm     Int.
    

        624.63   6.975     32
        624.00   6.968     37
        621.81   6.943     90
        620.06   6.924     75
        619.44   6.917    121
        618.81   6.910    130
        618.13   6.902    132
        617.38   6.894    179
        616.69   6.886    207
        616.00   6.879    206
        613.75   6.853     69
        602.06   6.723    268
        598.50   6.683     40
        596.94   6.666     37
        593.31   6.625    117
        558.19   6.233     36
        551.81   6.162     70
        548.69   6.127     37
        545.63   6.093     41
        542.38   6.057     74
        540.63   6.037     52
        536.19   5.987     45
        534.31   5.966     98
        531.13   5.931     77
        528.13   5.897     57
        524.81   5.860    132
        518.69   5.792     78
        470.44   5.253     34
        468.44   5.231    113
        466.81   5.213    220
        465.31   5.196    172
        463.94   5.181    216
        462.50   5.165    110
        462.00   5.159     83
        460.63   5.144     37
        455.94   5.091     48
        454.44   5.075    101
        453.94   5.069     69
        452.94   5.058    108
        452.50   5.053    147
        451.25   5.039    167
        449.31   5.017    104
        447.69   4.999     50
        303.94   3.394    182
        302.50   3.378    111
        299.13   3.340     96
        297.63   3.324    171
        296.25   3.308     99
        201.06   2.245   1000
    

in CDCl3



liquid film



4880 A,200 M,liquid