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网站主页CAS数据库列表 6609-64-9更多图谱2-氯-2-氧-1,3,2-二氧磷杂环戊烷(6609-64-9)质谱(MS)

2-氯-2-氧-1,3,2-二氧磷杂环戊烷

产品名称 2-氯-2-氧-1,3,2-二氧磷杂环戊烷

CAS号6609-64-9

分子式C2H4ClO3P

分子量142.48

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  • Mass

    MS-IW-9240          
    2-chloro-1,3,2-dioxaphospholane 2-oxide
    C2H4ClO3P           (Mass of molecular ion:    142)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          14.0       1.1
          15.0       9.7
          26.0       2.9
          27.0      12.0
          28.0       7.8
          29.0      11.2
          30.0       3.7
          31.0      11.9
          36.0       3.0
          38.0       1.0
          42.0      36.6
          43.0      23.3
          44.0     100.0
          45.0       2.5
          47.0      29.7
          48.0      12.7
          49.0       2.9
          61.0       1.0
          62.0      16.2
          63.0       8.1
          64.0       5.8
          65.0       2.6
          66.0       1.2
          77.0      18.4
          78.0       2.0
          79.0       3.2
          81.0      35.1
          82.0       1.6
          83.0      32.6
          84.0       8.9
          85.0      10.7
          86.0       2.6
          91.0       1.4
          99.0       3.8
         100.0       5.1
         101.0       2.0
         102.0       1.5
         106.0       2.7
         107.0      84.0
         108.0       2.1
         112.0      87.0
         113.0       7.1
         114.0      34.2
         115.0       2.5
         116.0       2.8
         117.0       4.2
         119.0       2.6
         135.0       3.1
         137.0       2.1
         141.0       6.2
         142.0      22.6
         143.0       4.6
         144.0       7.5
         145.0       1.0
         147.0       5.9
         149.0       3.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C2 H4 Cl O3 P 0.05 ml : 0.5 ml CDCl3
    2-chloro-1,3,2-dioxaphospholane 2-oxide
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 4.624 B *1 4.545

         Hz     ppm     Int.
    

       1875.37   4.693     53
       1868.16   4.675    352
       1862.43   4.661    456
       1861.45   4.658    634
       1860.96   4.657    514
       1857.54   4.648    538
       1855.59   4.644    502
       1852.54   4.636    758
       1848.51   4.626    495
       1845.83   4.619    445
       1845.21   4.618    578
       1843.99   4.615    721
       1842.53   4.611    343
       1841.06   4.607    548
       1839.11   4.602    531
       1836.43   4.596    739
       1834.84   4.592    316
       1833.25   4.588    139
       1832.52   4.586    148
       1829.96   4.579    110
       1828.86   4.577    114
       1826.78   4.571    402
       1824.83   4.567    817
       1821.78   4.559    514
       1819.82   4.554    544
       1818.48   4.551    272
       1817.50   4.548    587
       1817.02   4.547    643
       1815.67   4.544   1000
       1812.99   4.537    512
       1810.91   4.532    532
       1809.94   4.529    269
       1809.20   4.527    515
       1807.98   4.524    674
       1806.76   4.521    483
       1806.15   4.520    380
       1804.08   4.515    137
       1802.00   4.509     73
       1800.05   4.505    293
       1793.82   4.489     43
    

in CDCl3



liquid film