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MS-IW-0603 2-bromo-3-pyridinol C5H4BrNO (Mass of molecular ion: 173)
Source Temperature: 120 °C Sample Temperature: 90 °C Direct, 75 eV
18.0 3.3 28.0 1.7 37.0 2.8 38.0 11.0 39.0 23.8 40.0 2.6 54.0 1.7 64.0 5.0 65.0 29.3 66.0 16.8 67.0 8.4 93.0 60.3 94.0 51.0 95.0 3.2 173.0 100.0 174.0 6.9 175.0 97.6 176.0 6.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C5 H4 Br N O 0.041 g : 0.5 ml DMSO-d6 2-bromo-3-pyridinol Assign. Shift(ppm)
A 10.82 B 7.862 C 7.304 D 7.272
Hz ppm Int.
4326.02 10.825 119 3145.15 7.870 679 3143.32 7.866 772 3140.76 7.859 649 3138.92 7.855 676 2925.72 7.321 326 2923.89 7.317 387 2921.32 7.310 41 2917.66 7.301 923 2915.83 7.296 862 2910.70 7.284 1000 2906.30 7.273 943 2902.64 7.263 370 2898.24 7.252 364
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