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网站主页CAS数据库列表 6591-63-5更多图谱硫酸奎尼丁二水合物(6591-63-5)核磁图(13CNMR)

硫酸奎尼丁二水合物

产品名称 硫酸奎尼丁二水合物

CAS号6591-63-5

分子式C20H26N2O6S

分子量422.5

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400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C20 H24 N2 O2 saturated in CDCl3
    quinidine sulfate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.625 B 7.815 C 7.571 D 7.254 E 7.132 F 6.9 G 6.438 J 5.930 K 5.13 L 5.11 M *1 4.25 N 3.873 P *1 3.41 to 3.320 Q 3.26 R 3.08 S 2.34 T 2.23 U 1.83 V 1.68 W 1.56 X 0.81 ASSIGNED BY H-H COSY.

         Hz     ppm     Int.
    

       3448.36   8.629    149
       3443.85   8.618    147
       3129.27   7.831     41
       3127.20   7.825    168
       3120.00   7.807     46
       3118.04   7.802    182
       3026.25   7.573    158
       3021.85   7.562    156
       2899.41   7.255    144
       2896.85   7.249    141
       2855.71   7.146    115
       2853.15   7.140    103
       2846.44   7.123    108
       2843.99   7.117     98
       2567.87   6.426    114
       2387.08   5.973     35
       2386.84   5.973     35
       2379.52   5.955     40
       2376.59   5.947     41
       2369.38   5.929     72
       2362.30   5.911     45
       2359.38   5.904     45
       2351.93   5.885     43
       2057.37   5.148    120
       2043.46   5.114    136
       2040.28   5.106    122
       2033.08   5.088    118
       1705.93   4.269     32
       1705.32   4.268     32
       1704.96   4.267     33
       1697.63   4.248     37
       1697.02   4.247     39
       1696.17   4.245     41
       1695.19   4.242     40
       1694.21   4.240     40
       1693.36   4.238     41
       1692.99   4.237     40
       1692.14   4.235     39
       1684.08   4.214     34
       1683.72   4.213     34
       1547.73   3.873   1000
       1360.11   3.404     30
       1359.74   3.403     30
       1349.61   3.377     78
       1338.13   3.349     84
       1337.65   3.348     84
       1330.32   3.329     30
       1327.51   3.322     45
       1326.90   3.321     46
       1308.72   3.275     40
       1298.95   3.251     77
       1289.67   3.227     48
       1289.31   3.227     48
       1237.30   3.096     43
       1234.25   3.089     32
       1228.03   3.073     35
       1227.66   3.072     35
       1225.10   3.066     41
        936.04   2.343     49
        935.67   2.342     48
        927.37   2.321     46
        901.73   2.257     35
        901.49   2.256     35
        889.77   2.227     48
        889.28   2.226     48
        888.79   2.224     47
        878.17   2.198     34
        731.08   1.830     77
        670.41   1.678     39
        670.04   1.677     40
        669.31   1.675     41
        668.95   1.674     41
        668.58   1.673     41
        668.09   1.672     40
        665.65   1.666     33
        634.52   1.588     30
        625.24   1.565     50
        625.00   1.564     50
        623.66   1.561     49
        623.17   1.560     48
        614.14   1.537     39
        612.30   1.533     36
        328.74   0.823     57
        327.76   0.821     52
        326.17   0.817     58
        321.78   0.806     89
        318.85   0.798     38
        317.75   0.796     38
        317.02   0.794     39
        316.65   0.793     38
        315.92   0.791     38
        314.58   0.788     45
    

in CDCl3



KBr disc



nujol mull