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MassMS2015-05293CW N-methyl-1-naphthalenemethylamine hydrochloride C12H13N HCl (Mass of molecular ion: 171)
Source Temperature: 245 °C Sample Temperature: 20 °C Direct, 70 eV
28.0 1.8 36.0 7.3 38.0 2.4 39.0 1.0 42.0 16.7 43.0 2.4 44.0 16.8 50.0 1.0 51.0 1.8 57.5 1.2 62.0 1.0 63.0 3.5 65.0 1.2 70.5 1.0 74.0 1.6 75.0 2.2 76.0 1.5 77.0 3.7 78.0 1.3 83.5 3.5 84.5 4.4 85.5 4.1 87.0 1.4 89.0 2.8 91.0 1.0 101.0 1.7 102.0 2.3 113.0 1.8 114.0 1.2 115.0 24.2 116.0 2.6 126.0 4.7 127.0 13.5 128.0 25.2 129.0 11.0 130.0 4.7 139.0 14.8 140.0 4.0 141.0 80.9 142.0 64.3 143.0 7.2 153.0 2.7 154.0 7.7 155.0 2.1 156.0 3.7 166.0 1.0 167.0 2.1 168.0 7.5 169.0 3.9 170.0 100.0 171.0 86.0 172.0 10.6
in CDCl3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H13 N 0.038 g : 0.5 ml DMSO-d6 N-methyl-1-naphthalenemethylamine hydrochloride 
Assign. Shift(ppm)
A 9.70 B 8.274 C *1 8.02 D *1 8.01 E 7.834 F 7.63 G 7.58 J 7.57 K 4.630 L 2.650
Hz ppm Int.3877.41 9.703 96 3310.55 8.284 85 3303.38 8.266 79 3302.46 8.264 88 3208.77 8.029 89 3206.33 8.023 112 3205.41 8.021 111 3201.14 8.010 111 3199.31 8.006 105 3197.02 8.000 114 3135.07 7.845 93 3134.31 7.843 94 3128.05 7.827 110 3062.74 7.664 35 3061.22 7.660 42 3055.88 7.647 89 3054.35 7.643 85 3052.98 7.640 42 3047.94 7.627 116 3047.03 7.625 120 3045.96 7.622 125 3045.35 7.621 122 3040.01 7.607 52 3038.94 7.605 88 3037.72 7.601 90 3032.53 7.588 130 3030.85 7.584 45 3025.51 7.571 115 3024.44 7.568 115 3017.27 7.550 89 1850.74 4.631 411 1059.42 2.651 1000
in CDCl3
in DMSO-d6
KBr disc
nujol mull
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