22-二十三碳烯酸

Mass

MS-NW-9379          
22-tricosenoic acid
C23H44O2            (Mass of molecular ion:    352)

   Source Temperature: 240 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.5
      18.0       7.5
      27.0       4.1
      28.0       2.5
      29.0      15.2
      39.0       5.3
      40.0       1.0
      41.0      52.7
      42.0      10.0
      43.0      59.4
      44.0       2.1
      45.0       3.1
      53.0       3.2
      54.0      10.7
      55.0     100.0
      56.0      30.2
      57.0      55.4
      58.0       2.7
      59.0       2.5
      60.0      14.1
      61.0       3.3
      66.0       1.3
      67.0      18.4
      68.0      15.9
      69.0      76.0
      70.0      30.2
      71.0      26.0
      72.0       1.5
      73.0      16.0
      74.0       1.5
      79.0       2.6
      80.0       3.4
      81.0      19.5
      82.0      26.2
      83.0      68.9
      84.0      30.8
      85.0      15.7
      86.0       1.2
      87.0       4.5
      93.0       2.4
      94.0       4.7
      95.0      15.0
      96.0      27.1
      97.0      64.3
      98.0      29.4
      99.0       6.5
     100.0       2.7
     101.0       5.5
     107.0       2.5
     108.0       3.6
     109.0       9.4
     110.0      14.7
     111.0      32.0
     112.0      12.0
     113.0       4.3
     114.0       6.0
     115.0       4.7
     116.0       1.5
     119.0       1.8
     121.0       4.3
     122.0       2.7
     123.0       8.2
     124.0       9.7
     125.0      17.4
     126.0       6.7
     127.0       6.8
     128.0       1.7
     129.0       5.1
     133.0       2.0
     134.0       3.5
     135.0       4.7
     136.0       2.1
     137.0       6.7
     138.0       7.8
     139.0      10.3
     140.0       4.5
     141.0       2.2
     143.0       2.4
     147.0       1.8
     148.0       3.3
     149.0       3.5
     150.0       1.5
     151.0       5.7
     152.0       7.0
     153.0       6.8
     154.0       3.3
     155.0       1.7
     157.0       1.8
     161.0       1.5
     162.0       1.1
     163.0       2.1
     164.0       1.0
     165.0       4.2
     166.0       4.4
     167.0       4.5
     168.0       2.3
     169.0       1.5
     171.0       1.6
     175.0       1.2
     177.0       1.3
     179.0       3.3
     180.0       3.2
     181.0       3.1
     182.0       1.8
     183.0       1.1
     185.0       1.6
     193.0       2.7
     194.0       3.2
     195.0       2.3
     196.0       1.4
     207.0       2.6
     208.0       3.7
     209.0       1.9
     210.0       1.2
     221.0       2.8
     222.0       3.7
     223.0       1.5
     224.0       1.0
     235.0       3.0
     236.0       4.2
     237.0       1.4
     249.0       3.2
     250.0       4.9
     251.0       1.4
     263.0       3.1
     264.0       3.0
     277.0       2.6
     278.0       2.2
     290.0       1.7
     291.0       2.5
     292.0       4.0
     293.0       1.0
     305.0       1.4
     306.0       1.3
     316.0       1.4
     334.0      18.1
     335.0       5.0

Assign. Shift(ppm) A 11. B 5.811 C 4.990 D 4.925 E 2.345 F 2.038 G 1.628 J 1.37 K 1.26 J(B,C)=17.1HZ J(B,D)=10.3HZ J(B,F)=6.6HZ

     Hz     ppm     Int.

    944.91   2.365     36
    937.43   2.346     62
    929.74   2.327     39
    818.20   2.048     30
    500.88   1.254   1000